S_S-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate

Base Information

Chemical Name:S_S-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate
CAS No.:198342-81-3
Molecular Formula:C₂₇H₄₂O₇S
Molecular Weight:510.692
Hs Code.:

S<sub>S</sub>-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S_S-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate

Chemical Property:

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Technology Process of S_S-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate

There total 4 articles about S_S-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 582-52-5
1,2:5,6-di-O-isopropylidene-α-D-glucofuranose

: 198342-81-3
S_S-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate

: R_S-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate

Guidance literature:: With triethylamine; triphenylphosphine; In dichloromethane; at 0 ℃; for 1h; Product distribution; other phosphorus reagents; other solvents; var. temp. and reaction times;
DOI:10.1016/S0957-4166(99)00066-X

Reference yield:

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 198342-81-3
S_S-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / Zn / H₂O / 1 h / 90 °C

2: 1.) SOCl₂, 2.) pyridine / 1.) room temp., 3.5 h, 2.) Et₂O, room temp., overnight

With pyridine; thionyl chloride; zinc; In water;
DOI:10.1021/jo971093e

Reference yield:

: 717-74-8
1,3,5-triisopropyl benzene

: 198342-81-3
S_S-diacetone-D-glucosyl 2,4,6-triisopropylbenzenesulfinate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / ClSO₃H / CHCl₃ / 0 °C

2: 69 percent / Zn / H₂O / 1 h / 90 °C

3: 1.) SOCl₂, 2.) pyridine / 1.) room temp., 3.5 h, 2.) Et₂O, room temp., overnight

With pyridine; chlorosulfonic acid; thionyl chloride; zinc; In chloroform; water;
DOI:10.1021/jo971093e