Technology Process of C18H27NO6S
There total 4 articles about C18H27NO6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / water; 1,2-dichloro-ethane; aq. phosphate buffer / pH 8
2: camphor-10-sulfonic acid / 1,2-dichloro-ethane / 3 h / 20 °C
3: triethylamine; dmap / dichloromethane / 4 h / Cooling with ice
With
dmap; camphor-10-sulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
aq. phosphate buffer; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1021/jm400963y
- Guidance literature:
-
Multi-step reaction with 4 steps
1: lithium borohydride / tetrahydrofuran / 4 h / 20 °C
2: 3-chloro-benzenecarboperoxoic acid / water; 1,2-dichloro-ethane; aq. phosphate buffer / pH 8
3: camphor-10-sulfonic acid / 1,2-dichloro-ethane / 3 h / 20 °C
4: triethylamine; dmap / dichloromethane / 4 h / Cooling with ice
With
dmap; lithium borohydride; camphor-10-sulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; aq. phosphate buffer; dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1021/jm400963y
- Guidance literature:
-
Multi-step reaction with 2 steps
1: camphor-10-sulfonic acid / 1,2-dichloro-ethane / 3 h / 20 °C
2: triethylamine; dmap / dichloromethane / 4 h / Cooling with ice
With
dmap; camphor-10-sulfonic acid; triethylamine;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm400963y