(3-ethanesulfonyl-3,3-diphenyl-propyl)-dimethyl-amine; hydrochloride

Base Information

• Chemical Name: (3-ethanesulfonyl-3,3-diphenyl-propyl)-dimethyl-amine; hydrochloride
• CAS No.: 102321-34-6
• Molecular Formula: C₁₉H₂₅NO₂S*ClH
• Molecular Weight: 367.94
• Mol file: 102321-34-6.mol

Synonyms:

Chemical Property of (3-ethanesulfonyl-3,3-diphenyl-propyl)-dimethyl-amine; hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (3-ethanesulfonyl-3,3-diphenyl-propyl)-dimethyl-amine; hydrochloride

There total 3 articles about (3-ethanesulfonyl-3,3-diphenyl-propyl)-dimethyl-amine; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenylmethanethiol (4237-48-3) → (3-ethanesulfonyl-3,3-diphenyl-propyl)-dimethyl-amine; hydrochloride (102321-34-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium ethylate; ethanol / Eintragen von wss. H₂O₂ in eine Loesung des Reaktionsprodukts in Eisessig bei 60-80grad und anschliessendes Erhitzen auf 100grad

2: sodium amide; toluene

With ethanol; sodium ethanolate; sodium amide; toluene;

DOI:10.1021/ja01191a090

Reference yield:

diphenylchloromethane (90-99-3) → (3-ethanesulfonyl-3,3-diphenyl-propyl)-dimethyl-amine; hydrochloride (102321-34-6)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / Versetzen des Reaktionsgemisches mit wss. NaOH, anschliessendes Erhitzen auf Siedetemperatur

2: sodium ethylate; ethanol / Eintragen von wss. H₂O₂ in eine Loesung des Reaktionsprodukts in Eisessig bei 60-80grad und anschliessendes Erhitzen auf 100grad

3: sodium amide; toluene

With ethanol; sodium ethanolate; sodium amide; toluene;

DOI:10.1021/ja01191a090

Reference yield:

diphenylmethyl ethyl sulfone (6974-50-1) + 2-(dimethylamino)ethyl chloride (107-99-3) → (3-ethanesulfonyl-3,3-diphenyl-propyl)-dimethyl-amine; hydrochloride (102321-34-6)

Guidance literature:

With sodium amide; toluene;

DOI:10.1021/ja01191a090

upstream raw materials:

diphenylmethyl ethyl sulfone

2-(dimethylamino)ethyl chloride

diphenylmethanethiol

diphenylchloromethane