C₁₇H₁₈N₆O₆

Base Information

• Chemical Name: C₁₇H₁₈N₆O₆
• CAS No.: 1259314-16-3
• Molecular Formula: C₁₇H₁₈N₆O₆
• Molecular Weight: 402.367
• Mol file: 1259314-16-3.mol

Synonyms:

Chemical Property of C₁₇H₁₈N₆O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₁₈N₆O₆

There total 1 articles about C₁₇H₁₈N₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

chloro-trimethyl-silane (75-77-4) + 2-(azidomethyl)benzoyl chloride (289712-58-9) + CYTIDINE (65-46-3) → C17H18N6O6 (1259314-16-3)

Guidance literature:

chloro-trimethyl-silane; CYTIDINE; With pyridine; at 0 ℃; for 1h;

2-(azidomethyl)benzoyl chloride; With pyridine; at 20 ℃; for 3h;

DOI:10.1134/S1068162010050110

Reference yield: 89.0%

1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane (69304-37-6) + C17H18N6O6 (1259314-16-3) → C29H44N6O7Si2 (1259314-10-7)

Guidance literature:

With pyridine; at 20 ℃; for 16h;

DOI:10.1134/S1068162010050110

Reference yield:

C17H18N6O6 (1259314-16-3) → C52H48ClN10O13P

Guidance literature:

Multi-step reaction with 6 steps

1: pyridine / 16 h / 20 °C

2: acetic anhydride; acetic acid

3: tetrabutyl ammonium fluoride / tetrahydrofuran

4: 2-nitrobenzenesulfenyl chloride / N,N-dimethyl-formamide

5: pyridine / 2 h / 20 °C

6: pyridine; 2,4,6-triisopropylphenylsulfonyl chloride

With pyridine; 2,4,6-triisopropylphenylsulfonyl chloride; tetrabutyl ammonium fluoride; acetic anhydride; 2-nitrobenzenesulfenyl chloride; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1134/S1068162010050110

upstream raw materials:

chloro-trimethyl-silane

2-(azidomethyl)benzoyl chloride

CYTIDINE

Downstream raw materials:

C₁₈H₁₉N₉O₆

C₃₉H₃₇N₉O₈

C₂₉H₄₄N₆O₇Si₂