triphenylphosphine monohexylborane adduct

Base Information

• Chemical Name: triphenylphosphine monohexylborane adduct
• CAS No.: 87115-42-2
• Molecular Formula: C₆H₁₅B*C₁₈H₁₅P
• Molecular Weight: 360.287

Synonyms:

Chemical Property of triphenylphosphine monohexylborane adduct

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of triphenylphosphine monohexylborane adduct

There total 1 articles about triphenylphosphine monohexylborane adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

hexylidenetriphenylphosphorane-borane (79840-21-4) → triphenylphosphine monohexylborane adduct (87115-42-2)

Guidance literature:

In chlorobenzene; moisture and air-oxygen exclusion, heating (131°C, 25 min); solvent removal (room temp., high vacuum);

Reference yield:

Dichloromethyl methyl ether (4885-02-3) + triphenylphosphine monohexylborane adduct (87115-42-2) + 2,3-dimethyl-buta-1,3-diene (513-81-5) → 1-Hexyl-3,4-dimethyl-1-cyclopentanol (114672-84-3) + 1-Hexyl-3,4-dimethyl-1-cyclopentanol (79827-45-5) + 1-Hexyl-3,4-dimethyl-1-cyclopentanol (79895-96-8)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;

upstream raw materials:

hexylidenetriphenylphosphorane-borane

Downstream raw materials:

1-Hexyl-3,4-dimethyl-1-cyclopentanol

1-Hexyl-3,4-dimethyl-1-cyclopentanol

1-Hexyl-3,4-dimethyl-1-cyclopentanol

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