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hexylidenetriphenylphosphorane-borane

Base Information
  • Chemical Name:hexylidenetriphenylphosphorane-borane
  • CAS No.:79840-21-4
  • Molecular Formula:C24H30BP
  • Molecular Weight:360.287
  • Hs Code.:
hexylidenetriphenylphosphorane-borane

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Chemical Property of hexylidenetriphenylphosphorane-borane
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Technology Process of hexylidenetriphenylphosphorane-borane

There total 3 articles about hexylidenetriphenylphosphorane-borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In diethyl ether; moisture and air-oxygen exclusion, stirring (room temp., several hours), pptn.; BH3*THF, BH3-Et2S or BH3*1,4-oxathiane adducts also used (in place of BH3*SMe3); washing (ether), drying (high vacuum), recrystn. (acetone/water or CH2Cl2/ether); elem. anal.;
Guidance literature:
Aus Hexyl-triphenylphosphonium-bromid, 1) LiC6H5 in Ae. (N2, 1h), 2) B2H6;
DOI:10.1021/ja01463a026
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