2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-{2-[(2,3-dihydro-benzo[1,4]dioxin-2-ylmethyl)-methyl-amino]-ethyl} ester 5-isopropyl ester

Base Information

Chemical Name:2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-{2-[(2,3-dihydro-benzo[1,4]dioxin-2-ylmethyl)-methyl-amino]-ethyl} ester 5-isopropyl ester
CAS No.:119746-89-3
Molecular Formula:C₃₀H₃₅N₃O₈
Molecular Weight:565.623
Hs Code.:

2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-{2-[(2,3-dihydro-benzo[1,4]dioxin-2-ylmethyl)-methyl-amino]-ethyl} ester 5-isopropyl ester

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Chemical Property of 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-{2-[(2,3-dihydro-benzo[1,4]dioxin-2-ylmethyl)-methyl-amino]-ethyl} ester 5-isopropyl ester

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Technology Process of 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-{2-[(2,3-dihydro-benzo[1,4]dioxin-2-ylmethyl)-methyl-amino]-ethyl} ester 5-isopropyl ester

There total 3 articles about 2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-{2-[(2,3-dihydro-benzo[1,4]dioxin-2-ylmethyl)-methyl-amino]-ethyl} ester 5-isopropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 99-61-6
3-nitro-benzaldehyde

: 143093-33-8
isopropyl β-aminocrotonate

: 119747-01-2
1-Methyl-2-amino>ethyl acetoacetate

: 119746-89-3
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-{2-[(2,3-dihydro-benzo[1,4]dioxin-2-ylmethyl)-methyl-amino]-ethyl} ester 5-isopropyl ester

Guidance literature:: In isopropyl alcohol; Heating;
DOI:10.1021/jm00126a042

Reference yield:

: 2242-31-1
2-(N-methylaminomethyl)-2,3-dihydro-1,4-benzodioxin

: 119746-89-3
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-{2-[(2,3-dihydro-benzo[1,4]dioxin-2-ylmethyl)-methyl-amino]-ethyl} ester 5-isopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / triethylamine / toluene / Heating

2: 70 - 80 °C

3: 39 percent / propan-2-ol / Heating

With triethylamine; In isopropyl alcohol; toluene;
DOI:10.1021/jm00126a042

Reference yield:

: 73120-83-9
N-Methyl-N-(2-hydroxyethyl)(2,3-dihydro-1,4-benzodioxin-2-yl)methanamine

: 119746-89-3
2,6-Dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-{2-[(2,3-dihydro-benzo[1,4]dioxin-2-ylmethyl)-methyl-amino]-ethyl} ester 5-isopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 70 - 80 °C

2: 39 percent / propan-2-ol / Heating

In isopropyl alcohol;
DOI:10.1021/jm00126a042