[(bis(2-(i)Pr₂P-4-Me-phenyl)amido)Pd(tetrahydrofuran)][B(3,5-(CF₃)2C₆H₃)4]

Base Information

Chemical Name:[(bis(2-(i)Pr₂P-4-Me-phenyl)amido)Pd(tetrahydrofuran)][B(3,5-(CF₃)2C₆H₃)4]
CAS No.:1326316-48-6
Molecular Formula:C₃₀H₄₈NOP₂Pd*C₃₂H₁₂BF₂₄
Molecular Weight:1470.3
Hs Code.:

[(bis(2-(i)Pr<sub>2</sub>P-4-Me-phenyl)amido)Pd(tetrahydrofuran)][B(3,5-(CF<sub>3</sub>)2C<sub>6</sub>H<sub>3</sub>)4]

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Chemical Property of [(bis(2-(i)Pr₂P-4-Me-phenyl)amido)Pd(tetrahydrofuran)][B(3,5-(CF₃)2C₆H₃)4]

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Technology Process of [(bis(2-(i)Pr₂P-4-Me-phenyl)amido)Pd(tetrahydrofuran)][B(3,5-(CF₃)2C₆H₃)4]

There total 1 articles about [(bis(2-(i)Pr₂P-4-Me-phenyl)amido)Pd(tetrahydrofuran)][B(3,5-(CF₃)2C₆H₃)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 868135-72-2
(bis(2-(i)Pr₂P-4-Me-phenyl)amido)Pd(trifluoromethanesulfonate)

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 1326316-48-6
[(bis(2-(i)Pr₂P-4-Me-phenyl)amido)Pd(tetrahydrofuran)][B(3,5-(CF₃)2C₆H₃)4]

Guidance literature:: In tetrahydrofuran; under Ar; to a soln. of Pd-contg. compd. (0.10 mmol) in cold THF was added B-contg. compd. (0.10 mmol); stirring at room temp. for 1 h; the volatiles were removed under vac., the residue was dissolved in PhF;the mixt. was filtered through Celite; the filtrate was pumped to dryne ss; recrystn. from PhF/pentane; elem. anal.;
DOI:10.1021/ic2001283

Reference yield: 81.0%

: 1326316-48-6
[(bis(2-(i)Pr₂P-4-Me-phenyl)amido)Pd(tetrahydrofuran)][B(3,5-(CF₃)2C₆H₃)4]

: 1333-74-0
hydrogen

: 1326316-51-1
[(bis(2-(i)Pr₂P-4-Me-phenyl)amidoH)Pd(tetrahydrofuran)][B(3,5-(CF₃)2C₆H₃)4]

Guidance literature:: In fluorobenzene; under Ar; Pd-contg. compd. (0.026 mmol) was dissolved in fluorobenzene in a Young NMR tube; H2 (1 atm) was introduced into the tube; the mixt. was allowed to stand at room temp. for 30 min; the volatiles were removed under vac., the residue was washed with hexanes; the solid was dried under vac.; elem. anal.;
DOI:10.1021/ic2001283

Reference yield: 59.0%

: 1326316-48-6
[(bis(2-(i)Pr₂P-4-Me-phenyl)amido)Pd(tetrahydrofuran)][B(3,5-(CF₃)2C₆H₃)4]

: 274-07-7
benzo[1,3,2]dioxaborole

: 1326316-51-1
[(bis(2-(i)Pr₂P-4-Me-phenyl)amidoH)Pd(tetrahydrofuran)][B(3,5-(CF₃)2C₆H₃)4]

: 1326316-54-4
[(bis(2-(i)Pr₂P-4-Me-phenyl)amido-catecholborane-H)Pd(H)][B(3,5-(CF₃)2C₆H₃)4]

Guidance literature:: With Et₃N; In toluene; under Ar; Pd-contg. compd. (0.029 mmol) was dissolved in toluene/trifluorotoluen followed by addn. of B-contg. compd. (0.029 mmol); the mixt. was allowed to stand at room temp. for 1 h; Et3N (0.007 mmol) was added; the volatiles were removed under vac., the residue was washed with trifluorotoluene/pentane; elem. anal.;
DOI:10.1021/ic2001283