C₂₄H₂₅F₂N₃O₃S

Base Information

Chemical Name:C₂₄H₂₅F₂N₃O₃S
CAS No.:1393847-43-2
Molecular Formula:C₂₄H₂₅F₂N₃O₃S
Molecular Weight:473.544
Hs Code.:

C<sub>24</sub>H<sub>25</sub>F<sub>2</sub>N<sub>3</sub>O<sub>3</sub>S

Synonyms:

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Chemical Property of C₂₄H₂₅F₂N₃O₃S

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Technology Process of C₂₄H₂₅F₂N₃O₃S

There total 13 articles about C₂₄H₂₅F₂N₃O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1393847-42-1
C₂₅H₃₂F₂N₂O₅

: 333-20-0
potassium thioacyanate

: 1393847-43-2
C₂₄H₂₅F₂N₃O₃S

Guidance literature:: With hydrogenchloride; water; In ethanol; for 5h; Reflux;
DOI:10.1021/op300012d

Reference yield:

: 1034001-13-2
methyl 6,8-difluoro-2H-chromen-3-yl-carbamate

: 1393847-43-2
C₂₄H₂₅F₂N₃O₃S

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / methanol / 20 h / 80 °C / 22502.3 Torr

2: water; potassium hydroxide / methanol / 24 h / Reflux

3: STAB-H / dichloromethane / 4 h / 20 - 25 °C

4: hydrogenchloride; water / ethanol / 5 h / Reflux

With hydrogenchloride; water; hydrogen; potassium hydroxide; In methanol; ethanol; dichloromethane;
DOI:10.1021/op300012d

Reference yield:

: 1151797-94-2
6,8-difluoro-2H-chromene-3-carboxamide

: 1393847-43-2
C₂₄H₂₅F₂N₃O₃S

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hypochlorite; sodium hydroxide / methanol / 24 h / 25 °C

2: hydrogen / methanol / 20 h / 80 °C / 22502.3 Torr

3: water; potassium hydroxide / methanol / 24 h / Reflux

4: STAB-H / dichloromethane / 4 h / 20 - 25 °C

5: hydrogenchloride; water / ethanol / 5 h / Reflux

With hydrogenchloride; sodium hypochlorite; water; hydrogen; potassium hydroxide; sodium hydroxide; In methanol; ethanol; dichloromethane; 1: Hofmann rearrangement;
DOI:10.1021/op300012d