Technology Process of 2-(4'-benzyloxybenzoyloxy)-3,4,6-trimethoxyacetophenone
There total 1 articles about 2-(4'-benzyloxybenzoyloxy)-3,4,6-trimethoxyacetophenone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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/BRN= 119262/, C6H5-CH2O-p-C6H4-COCl in Pyridin;
- Guidance literature:
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Multi-step reaction with 5 steps
1: KOH / pyridine / 0.33 h / 110 °C
2: conc. H2SO4 / acetic acid / 0.12 h / 110 °C
3: H2 / Pd-C
4: AlCl3 / nitrobenzene / Ambient temperature
5: K2CO3 / acetone / 5 h / Heating
With
potassium hydroxide; aluminium trichloride; sulfuric acid; hydrogen; potassium carbonate;
palladium on activated charcoal;
In
pyridine; acetic acid; nitrobenzene; acetone;
DOI:10.1248/cpb.28.717
- Guidance literature:
-
Multi-step reaction with 6 steps
1: KOH / pyridine / 0.33 h / 110 °C
2: conc. H2SO4 / acetic acid / 0.12 h / 110 °C
3: H2 / Pd-C
4: AlCl3 / nitrobenzene / Ambient temperature
5: K2CO3 / acetone / 5 h / Heating
6: AcONa / 1 h / Heating
With
potassium hydroxide; aluminium trichloride; sulfuric acid; hydrogen; sodium acetate; potassium carbonate;
palladium on activated charcoal;
In
pyridine; acetic acid; nitrobenzene; acetone;
DOI:10.1248/cpb.28.717