Technology Process of 6-Demethoxytangeretin
There total 20 articles about 6-Demethoxytangeretin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: H2 / Pd-C
2: AlCl3 / nitrobenzene / Ambient temperature
3: K2CO3 / acetone / 5 h / Heating
With
aluminium trichloride; hydrogen; potassium carbonate;
palladium on activated charcoal;
In
nitrobenzene; acetone;
DOI:10.1248/cpb.28.717
- Guidance literature:
-
Multi-step reaction with 6 steps
1: (CF3CO)2O / benzene / 4 h / Ambient temperature
2: KOH / pyridine / 0.33 h / 110 °C
3: conc. H2SO4 / acetic acid / 0.12 h / 110 °C
4: H2 / Pd-C
5: AlCl3 / nitrobenzene / Ambient temperature
6: K2CO3 / acetone / 5 h / Heating
With
potassium hydroxide; aluminium trichloride; sulfuric acid; hydrogen; potassium carbonate; trifluoroacetic anhydride;
palladium on activated charcoal;
In
pyridine; acetic acid; nitrobenzene; acetone; benzene;
DOI:10.1248/cpb.28.717
- Guidance literature:
-
Multi-step reaction with 6 steps
1: (CF3CO)2O / benzene / 4 h / Ambient temperature
2: KOH / pyridine / 0.33 h / 110 °C
3: conc. H2SO4 / acetic acid / 0.12 h / 110 °C
4: H2 / Pd-C
5: AlCl3 / nitrobenzene / Ambient temperature
6: K2CO3 / acetone / 5 h / Heating
With
potassium hydroxide; aluminium trichloride; sulfuric acid; hydrogen; potassium carbonate; trifluoroacetic anhydride;
palladium on activated charcoal;
In
pyridine; acetic acid; nitrobenzene; acetone; benzene;
DOI:10.1248/cpb.28.717