C₂₂H₂₂NOP

Base Information

Chemical Name:C₂₂H₂₂NOP
CAS No.:1323157-04-5
Molecular Formula:C₂₂H₂₂NOP
Molecular Weight:347.397
Hs Code.:

Synonyms:

Suppliers and Price of C₂₂H₂₂NOP

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₂NOP

Chemical Property:

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Technology Process of C₂₂H₂₂NOP

There total 5 articles about C₂₂H₂₂NOP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 142087-72-7
P-phenyl-P-(2,4,6-trimethylphenyl)phosphinamide

: 1323157-04-5
C₂₂H₂₂NOP

Guidance literature:: With titanium tetrachloride; triethylamine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201100380

Reference yield:

: 1323156-96-2
C₂₂H₂₄NOP

: 1323157-04-5
C₂₂H₂₂NOP

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 24 h / 20 °C / 15001.5 Torr / Autoclave

2: titanium tetrachloride; triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; titanium tetrachloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1002/ejoc.201100380

Reference yield:

: 98934-20-4
2,4,6-trimethylphenylphenylphosphine oxide

: 1323157-04-5
C₂₂H₂₂NOP

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

2.1: triethylamine / diethyl ether / 16 h / 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / ethanol / 24 h / 20 °C / 15001.5 Torr / Autoclave

4.1: titanium tetrachloride; triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

With palladium 10% on activated carbon; hydrogen; titanium tetrachloride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1002/ejoc.201100380