(2S)-N-<(1R)-1-carboxy-2-methylprop-2-enyl>-3,3-diethoxy-2-phenylacetamidopropionamide

Base Information

• Chemical Name: (2S)-N-<(1R)-1-carboxy-2-methylprop-2-enyl>-3,3-diethoxy-2-phenylacetamidopropionamide
• CAS No.: 89766-19-8
• Molecular Formula: C₂₀H₂₈N₂O₆
• Molecular Weight: 392.452

Synonyms:

Chemical Property of (2S)-N-<(1R)-1-carboxy-2-methylprop-2-enyl>-3,3-diethoxy-2-phenylacetamidopropionamide

Chemical Property:

Purity/Quality:

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Technology Process of (2S)-N-<(1R)-1-carboxy-2-methylprop-2-enyl>-3,3-diethoxy-2-phenylacetamidopropionamide

There total 4 articles about (2S)-N-<(1R)-1-carboxy-2-methylprop-2-enyl>-3,3-diethoxy-2-phenylacetamidopropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

methanol (67-56-1) + methyl (2R)-2-<(1S,5R)-3-benzyl-7-oxo-4-oxa-2,6-diazabicyclo<3.2.0>hept-2-en-6-yl>-3-methylbut-3-enoate (79434-35-8) → (R)-2-[(2-Benzyl-oxazole-4-carbonyl)-amino]-3-methyl-but-3-enoic acid methyl ester (89766-20-1) + (2S)-N-<(1R)-1-carboxy-2-methylprop-2-enyl>-3,3-diethoxy-2-phenylacetamidopropionamide (89766-19-8)

Guidance literature:

for 34h; Heating;

DOI:10.1248/cpb.31.4539

Reference yield: 35.0%

methyl (2R)-2-<(1S,5R)-3-benzyl-7-oxo-4-oxa-2,6-diazabicyclo<3.2.0>hept-2-en-6-yl>-3-methylbut-3-enoate (79434-35-8) → (R)-2-[(2-Benzyl-oxazole-4-carbonyl)-amino]-3-methyl-but-3-enoic acid methyl ester (89766-20-1) + (2S)-N-<(1R)-1-carboxy-2-methylprop-2-enyl>-3,3-diethoxy-2-phenylacetamidopropionamide (89766-19-8)

Guidance literature:

With methanol; for 34h; Heating;

DOI:10.1248/cpb.31.4539

Reference yield: 35.0%

ethanol (64-17-5) + (2R,5S,6S)-2-(1-methylethenyl)-6-phenylacetamido-4-oxa-1-azabicyclo<3.2.0>heptane-3,7-dione (79386-28-0) → 2-phenylmethyl-4--carbamoyloxazole (89766-15-4) + (3S,4S)-1-<(1R)-1-carboxy-2-methylprop-2-enyl>-4-ethoxy-3-phenylacetamidoazetidin-2-one (89766-18-7) + (2S)-N-<(1R)-1-carboxy-2-methylprop-2-enyl>-3,3-diethoxy-2-phenylacetamidopropionamide (89766-19-8)

Guidance literature:

for 1h; Heating;

DOI:10.1248/cpb.31.4539

upstream raw materials:

methanol

methyl (2R)-2-<(1S,5R)-3-benzyl-7-oxo-4-oxa-2,6-diazabicyclo<3.2.0>hept-2-en-6-yl>-3-methylbut-3-enoate

ethanol

(2R,5S,6S)-2-(1-methylethenyl)-6-phenylacetamido-4-oxa-1-azabicyclo<3.2.0>heptane-3,7-dione

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