-3-(1H-indol-3-ylmethyl)-3-methyl-4,9,12-trioxo-7-phenyl-14-oxa-2,5,8,13-tetraazapentadecanoic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

Base Information

• Chemical Name: -3-(1H-indol-3-ylmethyl)-3-methyl-4,9,12-trioxo-7-phenyl-14-oxa-2,5,8,13-tetraazapentadecanoic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester
• CAS No.: 141956-63-0
• Molecular Formula: C₃₆H₄₅N₅O₆
• Molecular Weight: 643.783

Synonyms:

Chemical Property of -3-(1H-indol-3-ylmethyl)-3-methyl-4,9,12-trioxo-7-phenyl-14-oxa-2,5,8,13-tetraazapentadecanoic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of -3-(1H-indol-3-ylmethyl)-3-methyl-4,9,12-trioxo-7-phenyl-14-oxa-2,5,8,13-tetraazapentadecanoic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester

There total 1 articles about -3-(1H-indol-3-ylmethyl)-3-methyl-4,9,12-trioxo-7-phenyl-14-oxa-2,5,8,13-tetraazapentadecanoic acid tricyclo<3.3.1.1^3,7>dec-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methoxylamine hydrochloride (593-56-6) + N-{(R)-2-[(R)-2-(Adamantan-2-yloxycarbonylamino)-3-(1H-indol-3-yl)-2-methyl-propionylamino]-1-phenyl-ethyl}-succinamic acid (130332-27-3) → -3-(1H-indol-3-ylmethyl)-3-methyl-4,9,12-trioxo-7-phenyl-14-oxa-2,5,8,13-tetraazapentadecanoic acid tricyclo<3.3.1.13,7>dec-2-yl ester (141956-63-0)

Guidance literature:

With 2,3,4,5,6-pentafluorophenol; triethylamine; dicyclohexyl-carbodiimide; Yield given. Multistep reaction; 1.) DMF, RT, 3 h, 2.) DMF, RT, 4 d;

DOI:10.1021/jm00092a007

upstream raw materials:

N-methoxylamine hydrochloride

N-{(R)-2-[(R)-2-(Adamantan-2-yloxycarbonylamino)-3-(1H-indol-3-yl)-2-methyl-propionylamino]-1-phenyl-ethyl}-succinamic acid

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