Technology Process of C26H38O10
There total 4 articles about C26H38O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 85 percent / diisopropyl ethylamine / CH2Cl2 / 4 h / Ambient temperature
2: 1.) Mg, I2 / 1.) THF, reflux, 1.5 h, 2.) THF, room temperature, 3 h
3: diisopropyl ethylamine / CH2Cl2 / 5 h / Ambient temperature
4: LiClO4, NaOAc / anodic oxidation at 1.3 V
With
iodine; sodium acetate; lithium perchlorate; magnesium; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
DOI:10.1016/S0040-4020(97)10196-X
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) Mg, I2 / 1.) THF, reflux, 1.5 h, 2.) THF, room temperature, 3 h
2: diisopropyl ethylamine / CH2Cl2 / 5 h / Ambient temperature
3: LiClO4, NaOAc / anodic oxidation at 1.3 V
With
iodine; sodium acetate; lithium perchlorate; magnesium; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
DOI:10.1016/S0040-4020(97)10196-X
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diisopropyl ethylamine / CH2Cl2 / 5 h / Ambient temperature
2: LiClO4, NaOAc / anodic oxidation at 1.3 V
With
sodium acetate; lithium perchlorate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
DOI:10.1016/S0040-4020(97)10196-X