(3E)-9-benzyloxy-4,8-dimethylnon-3-en-1-ol

Base Information

Chemical Name:(3E)-9-benzyloxy-4,8-dimethylnon-3-en-1-ol
CAS No.:100631-91-2
Molecular Formula:C₁₈H₂₈O₂
Molecular Weight:276.419
Hs Code.:

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Chemical Property of (3E)-9-benzyloxy-4,8-dimethylnon-3-en-1-ol

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Technology Process of (3E)-9-benzyloxy-4,8-dimethylnon-3-en-1-ol

There total 4 articles about (3E)-9-benzyloxy-4,8-dimethylnon-3-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2468-55-5
5-iodopent-1-yne

: 100631-91-2
(3E)-9-benzyloxy-4,8-dimethylnon-3-en-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) LDA, 2.) hexamethylphosphoramide / 1.) THF, -78 deg C, 1 h; 2.) THF, -78 deg C to room temperature, 15 h

2: 94 percent / lithium aluminium hydride / diethyl ether / 1.5 h / 0 °C

3: 85 percent / sodium hydride / dimethylformamide / 12 h / 0 - 20 °C

4: zirconiumbis(cyclopentadienyl) dichloride, n-Bu-Li

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; zirconocene dichloride; sodium hydride; lithium diisopropyl amide; In diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 100582-49-8
2-methylhept-6-yn-1-ol

: 100631-91-2
(3E)-9-benzyloxy-4,8-dimethylnon-3-en-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / sodium hydride / dimethylformamide / 12 h / 0 - 20 °C

2: zirconiumbis(cyclopentadienyl) dichloride, n-Bu-Li

With n-butyllithium; zirconocene dichloride; sodium hydride; In N,N-dimethyl-formamide;

Reference yield:

: 100582-48-7
t-butyl 2-methylhept-6-ynoate

: 100631-91-2
(3E)-9-benzyloxy-4,8-dimethylnon-3-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / lithium aluminium hydride / diethyl ether / 1.5 h / 0 °C

2: 85 percent / sodium hydride / dimethylformamide / 12 h / 0 - 20 °C

3: zirconiumbis(cyclopentadienyl) dichloride, n-Bu-Li

With lithium aluminium tetrahydride; n-butyllithium; zirconocene dichloride; sodium hydride; In diethyl ether; N,N-dimethyl-formamide;