Technology Process of 5-benzylideneamino-4-benzylidenehydrazino-2-t-butylpyrimidine
There total 6 articles about 5-benzylideneamino-4-benzylidenehydrazino-2-t-butylpyrimidine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 86 percent / aq. NaOH / Ambient temperature; overnight
2: 92 percent / KNO3, H2SO4 conc. / 8 h / 115 °C
3: POCl3 / 1) reflux, 3 h, 2) RT, overnight
4: 86 percent / NH2NH2*H2O / diethyl ether / 0.5 h / 0 °C
5: H2 / 5percent Pd/C / methanol / Ambient temperature
6: methanol / 48 h / Ambient temperature
With
sodium hydroxide; sulfuric acid; hydrogen; hydrazine hydrate; potassium nitrate; trichlorophosphate;
palladium on activated charcoal;
In
methanol; diethyl ether;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / NH2NH2*H2O / diethyl ether / 0.5 h / 0 °C
2: H2 / 5percent Pd/C / methanol / Ambient temperature
3: methanol / 48 h / Ambient temperature
With
hydrogen; hydrazine hydrate;
palladium on activated charcoal;
In
methanol; diethyl ether;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: H2 / 5percent Pd/C / methanol / Ambient temperature
2: methanol / 48 h / Ambient temperature
With
hydrogen;
palladium on activated charcoal;
In
methanol;
