Z-Phe-Gly-OMe

Base Information

Chemical Name:Z-Phe-Gly-OMe
CAS No.:708228-79-9
Molecular Formula:C₂₂H₂₇N₂O₈P
Molecular Weight:478.439
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Z-Phe-Gly-OMe

Chemical Property:

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Technology Process of Z-Phe-Gly-OMe

There total 6 articles about Z-Phe-Gly-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23828-09-3
N-(benzyloxycarbonyl)-L-phenylalanyl-L-serine methyl ester

: 708228-79-9
Z-Phe-Gly-OMe

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / molecular sieve 4A / ethyl acetate / Heating

2: 90 percent / diazabicyclo<2.2.2>octane / tetrahydrofuran / 1) 2 h, -78 deg C 2) to r.t., overnight

3: SO₂Cl₂ / ethyl acetate / 0.25 h / 0 °C

4: ethyl acetate / 1 h / Heating

With 1,4-diaza-bicyclo[2.2.2]octane; sulfuryl dichloride; 4 A molecular sieve; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/S0040-4039(00)79711-5

Reference yield:

: 872130-35-3
N-benzyloxycarbonyl-L-phenylalanyl-DL-α-acetoxyglycine methyl ester

: 708228-79-9
Z-Phe-Gly-OMe

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / diazabicyclo<2.2.2>octane / tetrahydrofuran / 1) 2 h, -78 deg C 2) to r.t., overnight

2: SO₂Cl₂ / ethyl acetate / 0.25 h / 0 °C

3: ethyl acetate / 1 h / Heating

With 1,4-diaza-bicyclo[2.2.2]octane; sulfuryl dichloride; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/S0040-4039(00)79711-5

Reference yield:

: 188302-22-9
N-benzyloxycarbonyl-L-phenylalanyl-DL-α-(ethylthio)glycine methyl ester

: 708228-79-9
Z-Phe-Gly-OMe

Guidance literature:: Multi-step reaction with 2 steps

1: SO₂Cl₂ / ethyl acetate / 0.25 h / 0 °C

2: ethyl acetate / 1 h / Heating

With sulfuryl dichloride; In ethyl acetate;
DOI:10.1016/S0040-4039(00)79711-5