(3-acetoxy-2-chloropropyl)phenylselenium dichloride

Base Information

• Chemical Name: (3-acetoxy-2-chloropropyl)phenylselenium dichloride
• CAS No.: 109391-92-6
• Molecular Formula: C₁₁H₁₃Cl₃O₂Se
• Molecular Weight: 362.542

Synonyms:

Chemical Property of (3-acetoxy-2-chloropropyl)phenylselenium dichloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-acetoxy-2-chloropropyl)phenylselenium dichloride

There total 4 articles about (3-acetoxy-2-chloropropyl)phenylselenium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Phenylselenyl chloride (5707-04-0) → (3-acetoxy-2-chloropropyl)phenylselenium dichloride (109391-92-6)

Guidance literature:

Multi-step reaction with 3 steps

1: CHCl₃ / 72 h / Ambient temperature

2: sulfuryl chloride / CHCl₃ / 2 h / Ambient temperature

3: CHCl₃ / 0.5 h / Heating

With sulfuryl dichloride; In chloroform;

DOI:10.1021/jo00227a026

Reference yield:

2-Chloro-2-phenylselanyl-ethanol → (3-acetoxy-2-chloropropyl)phenylselenium dichloride (109391-92-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuryl chloride / CHCl₃ / 2 h / Ambient temperature

2: CHCl₃ / 0.5 h / Heating

With sulfuryl dichloride; In chloroform;

DOI:10.1021/jo00227a026

Reference yield:

C8H9Cl3OSe + acetyl chloride (75-36-5) → (3-acetoxy-2-chloropropyl)phenylselenium dichloride (109391-92-6)

Guidance literature:

In chloroform; for 0.5h; Yield given; Heating;

DOI:10.1021/jo00227a026

upstream raw materials:

acetyl chloride

Phenylselenyl chloride

allyl alcohol

Downstream raw materials:

3-acetoxy-2-chloroprop-1-ene

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