1-(7-(benzyloxy)-1,1,2,2,3,3,4,4,5,5,6,6-dodecafluoroheptyl)-3-trifluoromethoxy benzene

Base Information

Chemical Name:1-(7-(benzyloxy)-1,1,2,2,3,3,4,4,5,5,6,6-dodecafluoroheptyl)-3-trifluoromethoxy benzene
CAS No.:1310492-08-0
Molecular Formula:C₂₁H₁₃F₁₅O₂
Molecular Weight:582.309
Hs Code.:

Synonyms:

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Chemical Property of 1-(7-(benzyloxy)-1,1,2,2,3,3,4,4,5,5,6,6-dodecafluoroheptyl)-3-trifluoromethoxy benzene

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Technology Process of 1-(7-(benzyloxy)-1,1,2,2,3,3,4,4,5,5,6,6-dodecafluoroheptyl)-3-trifluoromethoxy benzene

There total 3 articles about 1-(7-(benzyloxy)-1,1,2,2,3,3,4,4,5,5,6,6-dodecafluoroheptyl)-3-trifluoromethoxy benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 66790-20-3
((2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoroheptyloxy)methyl)benzene

: 198206-33-6
1-iodo-3-(trifluoromethoxy)benzene

: 1310492-08-0
1-(7-(benzyloxy)-1,1,2,2,3,3,4,4,5,5,6,6-dodecafluoroheptyl)-3-trifluoromethoxy benzene

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; 1,10-Phenanthroline; bis(2,2,6,6-tetramethyl-1-piperidyl)zinc; copper(l) chloride; at 60 - 90 ℃; for 13.25h;
DOI:10.1021/ja2041942

Reference yield:

: 100-39-0
benzyl bromide

: 1310492-08-0
1-(7-(benzyloxy)-1,1,2,2,3,3,4,4,5,5,6,6-dodecafluoroheptyl)-3-trifluoromethoxy benzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 16 h / 20 °C

2: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; 1,10-Phenanthroline; bis(2,2,6,6-tetramethyl-1-piperidyl)zinc; copper(l) chloride / 13.25 h / 60 - 90 °C

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; potassium phosphate; 1,10-Phenanthroline; bis(2,2,6,6-tetramethyl-1-piperidyl)zinc; tetra-(n-butyl)ammonium iodide; copper(l) chloride; In N,N-dimethyl-formamide;
DOI:10.1021/ja2041942

Reference yield:

: 335-99-9
2,2,3,3,4,4,5,5,6,6,7,7-dodecafluoro-1-heptanol

: 1310492-08-0
1-(7-(benzyloxy)-1,1,2,2,3,3,4,4,5,5,6,6-dodecafluoroheptyl)-3-trifluoromethoxy benzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium phosphate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 16 h / 20 °C

2: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; 1,10-Phenanthroline; bis(2,2,6,6-tetramethyl-1-piperidyl)zinc; copper(l) chloride / 13.25 h / 60 - 90 °C

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; potassium phosphate; 1,10-Phenanthroline; bis(2,2,6,6-tetramethyl-1-piperidyl)zinc; tetra-(n-butyl)ammonium iodide; copper(l) chloride; In N,N-dimethyl-formamide;
DOI:10.1021/ja2041942