C₂₁H₂₇NO₃

Base Information

Chemical Name:C₂₁H₂₇NO₃
CAS No.:1345336-02-8
Molecular Formula:C₂₁H₂₇NO₃
Molecular Weight:341.45
Hs Code.:

C<sub>21</sub>H<sub>27</sub>NO<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₇NO₃

Chemical Property:

Purity/Quality:

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Technology Process of C₂₁H₂₇NO₃

There total 1 articles about C₂₁H₂₇NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5375-00-8
3-benzyloxypropyl iodide

: 3081-24-1
H-Phe-OEt

: 1345336-02-8
C₂₁H₂₇NO₃

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃; Inert atmosphere;
DOI:10.1021/jo300887u

Reference yield:

: 1345336-02-8
C₂₁H₂₇NO₃

: C₁₄H₁₉NO₂

Guidance literature:: Multi-step reaction with 5 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / Inert atmosphere

2: palladium on activated charcoal; hydrogen / Inert atmosphere

3: carbon tetrabromide; triphenylphosphine / dichloromethane / Inert atmosphere

4: potassium hexamethylsilazane / N,N-dimethyl-formamide / 0.5 h / -60 °C / Inert atmosphere

5: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

With carbon tetrabromide; palladium on activated charcoal; hydrogen; potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo300887u

Reference yield:

: 1345336-02-8
C₂₁H₂₇NO₃

: C₂₁H₂₅NO₂

Guidance literature:: Multi-step reaction with 6 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / Inert atmosphere

2: palladium on activated charcoal; hydrogen / Inert atmosphere

3: carbon tetrabromide; triphenylphosphine / dichloromethane / Inert atmosphere

4: potassium hexamethylsilazane / N,N-dimethyl-formamide / 0.5 h / -60 °C / Inert atmosphere

5: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

6: tetra-(n-butyl)ammonium iodide; potassium carbonate / acetonitrile / 8 h / Inert atmosphere; Reflux

With carbon tetrabromide; palladium on activated charcoal; hydrogen; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; potassium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo300887u