C₅₆H₄₆O₆

Base Information

• Chemical Name: C₅₆H₄₆O₆
• CAS No.: 1377399-63-7
• Molecular Formula: C₅₆H₄₆O₆
• Molecular Weight: 814.978
• Mol file: 1377399-63-7.mol

Synonyms:

Chemical Property of C₅₆H₄₆O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₆H₄₆O₆

There total 4 articles about C₅₆H₄₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C21H16O6 + benzyl bromide (100-39-0) → C56H46O6 (1377399-63-7)

Guidance literature:

C₂₁H₁₆O₆; With sodium hydride; In N,N-dimethyl-formamide; at 25 ℃; for 0.0833333h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; at 25 ℃; for 3h; Inert atmosphere;

DOI:10.1002/anie.201107730

Reference yield:

(E)-[2,4-dimethoxy-6-(4-methoxystyryl)phenyl]-(3,5-dimethoxyphenyl)methanol (1001258-87-2) → C56H46O6 (1377399-63-7)

Guidance literature:

Multi-step reaction with 4 steps

1.1: Dess-Martin periodane / dichloromethane / 0.08 h / 25 °C

1.2: 1 h / 25 °C

2.1: toluene-4-sulfonic acid / toluene / 3 h / 80 °C / Inert atmosphere

3.1: boron tribromide / dichloromethane / 24 h / 40 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 25 °C / Inert atmosphere

4.2: 3 h / 25 °C / Inert atmosphere

With boron tribromide; sodium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1002/anie.201107730

Reference yield:

3,5,4'-trimethoxy-trans-stilbene (22255-22-7) → C56H46O6 (1377399-63-7)

Guidance literature:

Multi-step reaction with 6 steps

1.1: N-Bromosuccinimide / dichloromethane / 1 h / 25 °C / Inert atmosphere

2.1: n-butyllithium / Inert atmosphere

2.2: Inert atmosphere

3.1: Dess-Martin periodane / dichloromethane / 0.08 h / 25 °C

3.2: 1 h / 25 °C

4.1: toluene-4-sulfonic acid / toluene / 3 h / 80 °C / Inert atmosphere

5.1: boron tribromide / dichloromethane / 24 h / 40 °C / Inert atmosphere

6.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 25 °C / Inert atmosphere

6.2: 3 h / 25 °C / Inert atmosphere

With N-Bromosuccinimide; n-butyllithium; boron tribromide; sodium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1002/anie.201107730

upstream raw materials:

(E)-(2,4-dimethoxy-6-(4-methoxystyryl)phenyl)(3,5-dimethoxyphenyl)methanone

(E)-[2,4-dimethoxy-6-(4-methoxystyryl)phenyl]-(3,5-dimethoxyphenyl)methanol

benzyl bromide

3,5,4'-trimethoxy-trans-stilbene