(CH₂GeBr₂)3

Base Information

Chemical Name:(CH₂GeBr₂)3
CAS No.:124575-81-1
Molecular Formula:C₃H₆Br₆Ge₃
Molecular Weight:739.275
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (CH₂GeBr₂)3

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Technology Process of (CH₂GeBr₂)3

There total 1 articles about (CH₂GeBr₂)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 7440-56-4
germanium

: 74-95-3
1,1-dibromomethane

: 124575-81-1
(CH₂GeBr₂)3

: 124575-80-0
CH₂(GeBr₃)2

: 88511-99-3
Tribrom-brommethyl-german

: 1730-66-1
methylgermanium bromide

: 6558-57-2
methylgermyl tribromide

Guidance literature:: copper; under dried abs. N2; fine powdered Ge and Cu-Powder divided among glass wool in a quartz tube; addn. of CH2Br2 (1 drop/s) during heating in a oven until 310°C; reaction finished after 4 h; summarizing in cooling trap at -78°C; removing of excess CH2Br2 at 25°C and 1 atm; fractioned distn. under vac.; crystn. of (CH2GeBr2)2; elem. anal.; NMR; IR; mass spectroscopy;

upstream raw materials:

germanium

1,1-dibromomethane

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