(R)-3-{(R)-2-Carboxy-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-ethyldisulfanyl}-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-propionic acid

Base Information

Chemical Name:(R)-3-{(R)-2-Carboxy-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-ethyldisulfanyl}-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-propionic acid
CAS No.:39508-02-6
Molecular Formula:C₃₀H₄₀N₂O₁₂S₂
Molecular Weight:684.786
Hs Code.:

(R)-3-{(R)-2-Carboxy-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-ethyldisulfanyl}-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-propionic acid

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Chemical Property of (R)-3-{(R)-2-Carboxy-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-ethyldisulfanyl}-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-propionic acid

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Technology Process of (R)-3-{(R)-2-Carboxy-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-ethyldisulfanyl}-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-propionic acid

There total 5 articles about (R)-3-{(R)-2-Carboxy-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-ethyldisulfanyl}-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39507-96-5
3,5-dimethoxy-α,α-dimethyl benzyl alcohol

: 39508-02-6
(R)-3-{(R)-2-Carboxy-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-ethyldisulfanyl}-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: (i) Py, CH₂Cl₂, (ii) N₂H₄*H₂O, DMF

2: NaNO₂, AcOH / dioxane

3: (i) 2NMe₃>OH, MeOH, (ii) /BRN= 2471550/, Py

With acetic acid; sodium nitrite; In 1,4-dioxane;
DOI:10.1002/jlac.19727630118

Reference yield:

: 17275-82-0
ethyl 3,5-dimethoxybenzoate

: 39508-02-6
(R)-3-{(R)-2-Carboxy-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-ethyldisulfanyl}-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-propionic acid

Guidance literature:: Multi-step reaction with 4 steps

1: (i) Mg, Et₂O, (ii) /BRN= 2105670/

2: (i) Py, CH₂Cl₂, (ii) N₂H₄*H₂O, DMF

3: NaNO₂, AcOH / dioxane

4: (i) 2NMe₃>OH, MeOH, (ii) /BRN= 2471550/, Py

With acetic acid; sodium nitrite; In 1,4-dioxane;
DOI:10.1002/jlac.19727630118

Reference yield:

: 39508-00-4
3,5-dimethoxy-α,α-dimethylbenzylcarbazate

: 39508-02-6
(R)-3-{(R)-2-Carboxy-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-ethyldisulfanyl}-2-[1-(3,5-dimethoxy-phenyl)-1-methyl-ethoxycarbonylamino]-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: NaNO₂, AcOH / dioxane

2: (i) 2NMe₃>OH, MeOH, (ii) /BRN= 2471550/, Py

With acetic acid; sodium nitrite; In 1,4-dioxane;
DOI:10.1002/jlac.19727630118