Acetic acid (2R,3R,4R,5R)-4-acetoxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester

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Chemical Name:Acetic acid (2R,3R,4R,5R)-4-acetoxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester
CAS No.:87875-18-1
Molecular Formula:C₄₁H₃₉N₃O₁₁
Molecular Weight:749.774
Hs Code.:

Acetic acid (2R,3R,4R,5R)-4-acetoxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester

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Chemical Property of Acetic acid (2R,3R,4R,5R)-4-acetoxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester

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Technology Process of Acetic acid (2R,3R,4R,5R)-4-acetoxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester

There total 3 articles about Acetic acid (2R,3R,4R,5R)-4-acetoxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 20264-96-4
2-(4-nitrophenyl)ethyl iodide

: 87875-12-5
5'-O-(monomethoxytrityl)-2',3'-bis-O-(acetyl)uridine

: 87875-18-1
Acetic acid (2R,3R,4R,5R)-4-acetoxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester

Guidance literature:: DOI:10.1016/S0040-4039(00)88175-7

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 87875-18-1
Acetic acid (2R,3R,4R,5R)-4-acetoxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / SOCl₂, pyridine / 2 h / Heating

2: NaI / butan-2-one

3: 70 percent

With pyridine; thionyl chloride; sodium iodide; In butanone;
DOI:10.1016/S0040-4039(00)88175-7

Reference yield:

: 20264-95-3
2-(4-nitrophenyl)ethyl chloride

: 87875-18-1
Acetic acid (2R,3R,4R,5R)-4-acetoxy-2-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-5-{4-[2-(4-nitro-phenyl)-ethoxy]-2-oxo-2H-pyrimidin-1-yl}-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / butan-2-one

2: 70 percent

With sodium iodide; In butanone;
DOI:10.1016/S0040-4039(00)88175-7