1-(2-phenyl-ortho-carboran-1-yl)phenylacetic acid

Base Information

Chemical Name:1-(2-phenyl-ortho-carboran-1-yl)phenylacetic acid
CAS No.:145826-14-8
Molecular Formula:C₁₆H₂₂B₁₀O₂
Molecular Weight:354.459
Hs Code.:

Synonyms:

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Chemical Property of 1-(2-phenyl-ortho-carboran-1-yl)phenylacetic acid

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Technology Process of 1-(2-phenyl-ortho-carboran-1-yl)phenylacetic acid

There total 2 articles about 1-(2-phenyl-ortho-carboran-1-yl)phenylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 23836-03-5
2-benzyl-1-phenyl-ortho-carborane

: 124-38-9,18923-20-1
carbon dioxide

: 145826-14-8
1-(2-phenyl-ortho-carboran-1-yl)phenylacetic acid

Guidance literature:: With n-butyllithium; ammonium chloride; In diethyl ether; water; addn. of soln. of n-C4H9Li to stirred soln. of 2-benzyl-1-phenyl-ortho-carborane in anhyd. ether, stirring for 0.5 h, passing of dry CO2 throughsoln. for 40 min, addn. of satd. aq. soln. of NH4Cl; sepn. of org. layer, extn. with ether from aq. layer, combination of etheral layers, washing with soln. of NaHCO3 and water, drying over Na2SO4,removal of solvent in vac., recrystn. from n-heptane;
DOI:10.1023/A:1015572605520

Reference yield: 86.0%

: 1-phenyl-2-benzyllithium-o-carborane

: 124-38-9,18923-20-1
carbon dioxide

: 145826-14-8
1-(2-phenyl-ortho-carboran-1-yl)phenylacetic acid

Guidance literature:: Ar; 20°C; heating;; elem. anal.;;
DOI:10.1007/BF00869528

Reference yield: 85.0%

: 67-56-1
methanol

: 145826-14-8
1-(2-phenyl-ortho-carboran-1-yl)phenylacetic acid

: 469866-36-2
methyl 1-(2-phenyl-ortho-carboran-1-yl)phenylacetate

Guidance literature:: With sulfuric acid; In methanol; (Ar); dissolving of 1-(2-phenyl-ortho-carboran-1-yl)phenylacetic acid in anhyd. MeOH, addn. of concd. H2SO4, reflux for 96 h without access foratmospheric moisture; pptn., filtration, recrystn. from MeOH, elem. anal.;
DOI:10.1023/A:1015572605520