{[2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylcarbamoyl]-tert-butoxycarbonylamino-methyl}-phosphonic acid dimethyl ester

Base Information

Chemical Name:{[2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylcarbamoyl]-tert-butoxycarbonylamino-methyl}-phosphonic acid dimethyl ester
CAS No.:132245-92-2
Molecular Formula:C₃₅H₅₈N₃O₁₀PSeSi₂
Molecular Weight:846.964
Hs Code.:

{[2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylcarbamoyl]-tert-butoxycarbonylamino-methyl}-phosphonic acid dimethyl ester

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Chemical Property of {[2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylcarbamoyl]-tert-butoxycarbonylamino-methyl}-phosphonic acid dimethyl ester

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Technology Process of {[2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylcarbamoyl]-tert-butoxycarbonylamino-methyl}-phosphonic acid dimethyl ester

There total 11 articles about {[2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylcarbamoyl]-tert-butoxycarbonylamino-methyl}-phosphonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 121056-96-0
(±)-2-((tert-butoxycarbonyl)amino)-2-(dimethoxyphosphoryl)acetic acid

: 132268-35-0
2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylamine

: 132245-92-2,132268-36-1
{[2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylcarbamoyl]-tert-butoxycarbonylamino-methyl}-phosphonic acid dimethyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/S0040-4039(00)97256-3

Reference yield:

: 51694-22-5
ortho-nitrophenyl selenocyanate

: 132245-92-2,132268-36-1
{[2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylcarbamoyl]-tert-butoxycarbonylamino-methyl}-phosphonic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / n-Bu₃P / tetrahydrofuran

2: 100 percent / 30percent TFA / CH₂Cl₂

3: 85 percent / DCC / CH₂Cl₂

With tributylphosphine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(00)97256-3

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 132245-92-2,132268-36-1
{[2-[3,4-Bis-(tert-butyl-dimethyl-silanyloxy)-phenyl]-2-(2-nitro-phenylselanyl)-ethylcarbamoyl]-tert-butoxycarbonylamino-methyl}-phosphonic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / CH₂Cl₂

2: 77 percent / 1N KOH / methanol

3: 85 percent / DCC / CH₂Cl₂

With potassium hydroxide; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1016/S0040-4039(00)97256-3