Fe2(CO)6(μ-C6H4-4-OH)2 * C6H6

Base Information

• Chemical Name: Fe2(CO)6(μ-C6H4-4-OH)2 * C6H6
• CAS No.: 168069-10-1
• Molecular Formula: C₆H₆*C₁₈H₁₀Fe₂O₈S₂
• Molecular Weight: 608.212
• Mol file: 168069-10-1.mol

Synonyms:

Chemical Property of Fe2(CO)6(μ-C6H4-4-OH)2 * C6H6

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Fe2(CO)6(μ-C6H4-4-OH)2 * C6H6

There total 2 articles about Fe2(CO)6(μ-C6H4-4-OH)2 * C6H6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

triiron dodecarbonyl (17685-52-8) + 4-sulfanylphenol (637-89-8) → Fe2(CO)6(μ-C6H4-4-OH)2 * C6H6 (168069-10-1)

Guidance literature:

In tetrahydrofuran; Ar-atmosphere; excess of ligand, refluxing for 2 h; removal of volatiles (vac.), trituration with pentane, dissoln. in ether, filtration through Florisil, evapn. (vac.), crystn. (C6H6); elem. anal.;

DOI:10.1021/ic00126a010

Reference yield:

triiron dodecarbonyl (17685-52-8) + bis(4-hydroxyphenyl)disulfide (15015-57-3) → Fe2(CO)6(μ-C6H4-4-OH)2 * C6H6 (168069-10-1)

Guidance literature:

In not given; Ar-atmosphere; recrystn. from C6H6;

DOI:10.1021/ic00126a010

Reference yield:

Fe2(CO)6(μ-C6H4-4-OH)2 * C6H6 (168069-10-1) + 4-sulfanylphenol (637-89-8) → Fe2(CO)6(μ-C6H4-4-OH)2 * 2HSC6H4OH

Guidance literature:

In toluene; Ar-atmosphere; crystn.; elem. anal.;

DOI:10.1021/ic00126a010

upstream raw materials:

triiron dodecarbonyl

bis(4-hydroxyphenyl)disulfide

4-sulfanylphenol