N-tosylactinobolamine methyl acetal

Base Information

Chemical Name:N-tosylactinobolamine methyl acetal
CAS No.:131895-70-0
Molecular Formula:C₁₇H₂₃NO₅S
Molecular Weight:353.439
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-tosylactinobolamine methyl acetal

Chemical Property:

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Technology Process of N-tosylactinobolamine methyl acetal

There total 14 articles about N-tosylactinobolamine methyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 67-56-1
methanol

: 131895-69-7,132015-15-7
(1R,4R,6R,8R,9R)-4-Methyl-2-(toluene-4-sulfonyl)-5-oxa-2-aza-tricyclo[4.3.1.0^3,8]decane-6,9-diol

: 131895-70-0
N-tosylactinobolamine methyl acetal

Guidance literature:: With toluene-4-sulfonic acid;
DOI:10.1039/c39900001412

Reference yield:

: 89366-20-1
methyl glyoxylate N-tosylhydrazone

: 131895-70-0
N-tosylactinobolamine methyl acetal

Guidance literature:: Multi-step reaction with 14 steps

1: 80 percent / toluene / Heating

2: 89 percent / m-chloroperoxybenzoic acid (m-CPBA) / CH₂Cl₂ / Heating

3: 92 percent / benzene; CH₂Cl₂ / Heating

4: TsOH / CH₂Cl₂ / 0 °C

5: DIBAL / CH₂Cl₂ / 0 °C

6: t-BuOK / dimethylsulfoxide

7: (COCl)2, DMSO

8: I₂, H₂O / dimethylsulfoxide

9: 97 percent / Bu₃SnH, azoisobutyronitrile / toluene / Heating

10: DIBAL / CH₂Cl₂

11: (COCl)2, DMSO

12: 81 percent / tetrahydrofuran / -30 °C

13: TsOH / tetrahydrofuran / Heating

14: 99 percent / TsOH

With oxalyl dichloride; 2,2'-azobis(isobutyronitrile); potassium tert-butylate; water; iodine; tri-n-butyl-tin hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; benzene;
DOI:10.1039/c39900001412

Reference yield:

: 89357-85-7,132015-11-3
(1S,3S,4R)-2-(Toluene-4-sulfonyl)-2-aza-bicyclo[2.2.2]oct-5-ene-3-carboxylic acid methyl ester

: 131895-70-0
N-tosylactinobolamine methyl acetal

Guidance literature:: Multi-step reaction with 13 steps

1: 89 percent / m-chloroperoxybenzoic acid (m-CPBA) / CH₂Cl₂ / Heating

2: 92 percent / benzene; CH₂Cl₂ / Heating

3: TsOH / CH₂Cl₂ / 0 °C

4: DIBAL / CH₂Cl₂ / 0 °C

5: t-BuOK / dimethylsulfoxide

6: (COCl)2, DMSO

7: I₂, H₂O / dimethylsulfoxide

8: 97 percent / Bu₃SnH, azoisobutyronitrile / toluene / Heating

9: DIBAL / CH₂Cl₂

10: (COCl)2, DMSO

11: 81 percent / tetrahydrofuran / -30 °C

12: TsOH / tetrahydrofuran / Heating

13: 99 percent / TsOH

With oxalyl dichloride; 2,2'-azobis(isobutyronitrile); potassium tert-butylate; water; iodine; tri-n-butyl-tin hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene; benzene;
DOI:10.1039/c39900001412