1-(4'-cyanobiphenyl-4-yl)-1'-octanoylferrocene

Base Information

Chemical Name:1-(4'-cyanobiphenyl-4-yl)-1'-octanoylferrocene
CAS No.:871732-72-8
Molecular Formula:C₃₁H₃₁FeNO
Molecular Weight:489.44
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4'-cyanobiphenyl-4-yl)-1'-octanoylferrocene

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Technology Process of 1-(4'-cyanobiphenyl-4-yl)-1'-octanoylferrocene

There total 1 articles about 1-(4'-cyanobiphenyl-4-yl)-1'-octanoylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 401845-44-1
1-(4'-cyanobiphenyl-4-yl)-ferrocene

: 111-64-8
n-octanoic acid chloride

: 871732-72-8
1-(4'-cyanobiphenyl-4-yl)-1'-octanoylferrocene

Guidance literature:: With AlCl₃; In dichloromethane; at 20°C under Ar atm.; mixt. of AlCl3, CH2Cl2 and C7H15COCl stirred for 1.5 h, then added dropwise to soln. of Fe-complex (ratio Fe-complex:C7H15COCl:AlCl3=1.0:1.0:1.4), stirred for 3 h, poured onto ice, concd. HCl and CHCl3 added; org. layer septd., washed (water), dried (MgSO4), filtered, solvent removed in vacuo, twice chromatographed on Al2O3, eluted with 1:1 CHCl3:light petroleum, solvent distd. off, recrystd. from light petroleum with small amt. of C6H6; elem. anal.;
DOI:10.1007/s11172-005-0053-6