iodido(1,4,7,10-tetraoxacyclotridec-12-ylmethyl)diphenylstannane

Base Information

Chemical Name:iodido(1,4,7,10-tetraoxacyclotridec-12-ylmethyl)diphenylstannane
CAS No.:1242843-57-7
Molecular Formula:C₂₂H₂₉IO₄Sn
Molecular Weight:603.084
Hs Code.:

Synonyms:

Suppliers and Price of iodido(1,4,7,10-tetraoxacyclotridec-12-ylmethyl)diphenylstannane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of iodido(1,4,7,10-tetraoxacyclotridec-12-ylmethyl)diphenylstannane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of iodido(1,4,7,10-tetraoxacyclotridec-12-ylmethyl)diphenylstannane

There total 1 articles about iodido(1,4,7,10-tetraoxacyclotridec-12-ylmethyl)diphenylstannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1242843-56-6
(1,4,7,10-tetraoxacyclotridec-12-ylmethyl)triphenylstannane

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 1242843-57-7
iodido(1,4,7,10-tetraoxacyclotridec-12-ylmethyl)diphenylstannane

Guidance literature:: In dichloromethane; byproducts: C6H5I; (N2 or Ar); I2 added over a period of 3 h at 0°C to a soln. of Sncompd., stirred and warmed to room temp. overnight; concd. (vac.), dissolved in EtOH, pptd. at -5°C; elem. anal.;
DOI:10.1021/om100409v

Reference yield: 51.0%

: 7789-23-3
potassium fluoride

: 1242843-57-7
iodido(1,4,7,10-tetraoxacyclotridec-12-ylmethyl)diphenylstannane

: 1242843-59-9
fluorido(1,4,7,10-tetraoxacyclotridec-12-ylmethyl)diphenylstannane

Guidance literature:: In dichloromethane; water; byproducts: KI; (N2 or Ar); a soln. of Sn compd. in CH2Cl2 mixed with an aq. soln. of KF, stirred at room temp. for 2 d; the org. phase sepd., dried (MgSO4), filtered, evapd. (vac.), dissolved in Et2O, pptd. at -5°C; elem. anal.;
DOI:10.1021/om100409v