1,12-PhCB₁₀H₁₀CC₆F₅

Base Information

Chemical Name:1,12-PhCB₁₀H₁₀CC₆F₅
CAS No.:265987-30-2
Molecular Formula:C₁₄H₁₅B₁₀F₅
Molecular Weight:386.375
Hs Code.:

1,12-PhCB<sub>10</sub>H<sub>10</sub>CC<sub>6</sub>F<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,12-PhCB₁₀H₁₀CC₆F₅

Chemical Property:

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Technology Process of 1,12-PhCB₁₀H₁₀CC₆F₅

There total 1 articles about 1,12-PhCB₁₀H₁₀CC₆F₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 392-56-3
Hexafluorobenzene

: 53065-73-9
1-phenyl-1,12-dicarba-closo-dodecaborane

: 265987-30-2
1,12-PhCB₁₀H₁₀CC₆F₅

: 265987-31-3
1,4-(p-PhCB₁₀H₁₀C)2C₆F₄

Guidance literature:: With n-C₄H₉Li; In diethyl ether; hexane; 1-Ph-p-carborane in dry Et2O added slowly with n-C4H9Li in hexane at 0°C under N2, warmed to room temp. with stirring, added dropwise toC6F6 (excess) in Et2O at 0°C, stirred for 24 h at room temp.; washed with dild. acid, filtered, insol. solid filtered off, ether layer washed, dried, solvent removed, combined with the insol. solid, extd. (hot MeCN), crystd. on cooling; elem. anal.;
DOI:10.1016/S0022-328X(99)00672-5

Reference yield: 79.0%

: 64-17-5
ethanol

: 265987-30-2
1,12-PhCB₁₀H₁₀CC₆F₅

: 265987-34-6
1-(p-PhCB₁₀H₁₀C)-4-EtOC₆F₄

Guidance literature:: With KOH; In diethyl ether; ethanol; PhCB10H10CC6F5 dissolved in Et2O/EtOH, added with KOH/EtOH, stirred at 50°C; solvent removed, dissolved in ether, washed, dried, solvent removed, recrystd. (CHCl3); elem. anal.;
DOI:10.1016/S0022-328X(99)00672-5

Reference yield: 72.0%

: 265987-30-2
1,12-PhCB₁₀H₁₀CC₆F₅

: 265987-33-5
1-(p-PhCB₁₀H₁₀C)-4-HOC₆F₄

Guidance literature:: With KOH; In tetrahydrofuran; refluxed for 30 min; evapd. (vac.), added with Et2O and dild. acid, ether layer sepd., washed, dried, solvent removed; elem. anal.;
DOI:10.1016/S0022-328X(99)00672-5