cis-(2R,6R)-2-methyl-6-((E)-2,4,6-trimethylstyryl)tetrahydropyran

Base Information

Chemical Name:cis-(2R,6R)-2-methyl-6-((E)-2,4,6-trimethylstyryl)tetrahydropyran
CAS No.:1314532-33-6
Molecular Formula:C₁₇H₂₄O
Molecular Weight:244.377
Hs Code.:

Synonyms:

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Chemical Property of cis-(2R,6R)-2-methyl-6-((E)-2,4,6-trimethylstyryl)tetrahydropyran

Chemical Property:

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Technology Process of cis-(2R,6R)-2-methyl-6-((E)-2,4,6-trimethylstyryl)tetrahydropyran

There total 4 articles about cis-(2R,6R)-2-methyl-6-((E)-2,4,6-trimethylstyryl)tetrahydropyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 852065-86-2
(R)-6-hepten-2-ol acetate

: 1314532-33-6
cis-(2R,6R)-2-methyl-6-((E)-2,4,6-trimethylstyryl)tetrahydropyran

Guidance literature:: Multi-step reaction with 3 steps

1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 40 °C

2: sodium methylate / methanol / 30 h / 20 °C

3: iron(III) chloride hexahydrate / dichloromethane / 1 h / 20 °C

With Hoveyda-Grubbs catalyst second generation; iron(III) chloride hexahydrate; sodium methylate; In methanol; dichloromethane;
DOI:10.1016/j.tet.2011.03.112

Reference yield:

: 1221972-05-9
acetic acid 1-(2,4,6-trimethyl-phenyl)-allyl ester

: 1314532-33-6
cis-(2R,6R)-2-methyl-6-((E)-2,4,6-trimethylstyryl)tetrahydropyran

Guidance literature:: Multi-step reaction with 3 steps

1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 40 °C

2: sodium methylate / methanol / 30 h / 20 °C

3: iron(III) chloride hexahydrate / dichloromethane / 1 h / 20 °C

With Hoveyda-Grubbs catalyst second generation; iron(III) chloride hexahydrate; sodium methylate; In methanol; dichloromethane;
DOI:10.1016/j.tet.2011.03.112

Reference yield:

: 487-68-3
mesytaldehyde

: 1314532-33-6
cis-(2R,6R)-2-methyl-6-((E)-2,4,6-trimethylstyryl)tetrahydropyran

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / -78 - 20 °C

1.2: 0 - 20 °C

2.1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 40 °C

3.1: sodium methylate / methanol / 30 h / 20 °C

4.1: iron(III) chloride hexahydrate / dichloromethane / 1 h / 20 °C

With Hoveyda-Grubbs catalyst second generation; iron(III) chloride hexahydrate; sodium methylate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tet.2011.03.112