bis(phenylhydrazino)phenylborane

Base Information

• Chemical Name: bis(phenylhydrazino)phenylborane
• CAS No.: 13831-66-8
• Molecular Formula: C₁₈H₁₉BN₄
• Molecular Weight: 302.187

Synonyms:

Chemical Property of bis(phenylhydrazino)phenylborane

Chemical Property:

Purity/Quality:

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Technology Process of bis(phenylhydrazino)phenylborane

There total 3 articles about bis(phenylhydrazino)phenylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

phenylbis(diethylamino)borane (887-60-5) + phenylhydrazine (100-63-0) → bis(phenylhydrazino)phenylborane (13831-66-8)

Guidance literature:

In Petroleum ether; heating for 1 h with reflux;

Reference yield: 42.0%

Bis-(dimethylamino)-phenylboran (1201-45-2) + phenylhydrazine (100-63-0) → bis(phenylhydrazino)phenylborane (13831-66-8)

Guidance literature:

In benzene; 6 h, reflux; pptn. with pentane, recrystn. from petroleum ether, pentane;

Reference yield: 36.0%

Bis-(dimethylamino)-phenylboran (1201-45-2) + phenylhydrazine (100-63-0) → bis(phenylhydrazino)phenylborane (13831-66-8) + Dimethylamino-phenylhydrazino-phenyl-boran (22072-67-9)

Guidance literature:

With C₆H₅NHNH₂; In xylene; byproducts: HN(CH3)2; 25°C for several h;

upstream raw materials:

Bis-(dimethylamino)-phenylboran

phenylhydrazine

phenylbis(diethylamino)borane

Downstream raw materials:

Perhydro-1,3,4,6-tetraphenyl-1,2,4,5-tetra-aza-1,3-diborin

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