Perhydro-1,3,4,6-tetraphenyl-1,2,4,5-tetra-aza-1,3-diborin

Base Information

• Chemical Name: Perhydro-1,3,4,6-tetraphenyl-1,2,4,5-tetra-aza-1,3-diborin
• CAS No.: 13831-67-9
• Molecular Formula: C₂₄H₂₂B₂N₄
• Molecular Weight: 388.087
• Mol file: 13831-67-9.mol

Synonyms:

Chemical Property of Perhydro-1,3,4,6-tetraphenyl-1,2,4,5-tetra-aza-1,3-diborin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Perhydro-1,3,4,6-tetraphenyl-1,2,4,5-tetra-aza-1,3-diborin

There total 5 articles about Perhydro-1,3,4,6-tetraphenyl-1,2,4,5-tetra-aza-1,3-diborin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

bis(phenylhydrazino)phenylborane (13831-66-8) → Perhydro-1,3,4,6-tetraphenyl-1,2,4,5-tetra-aza-1,3-diborin (13831-67-9)

Guidance literature:

byproducts: C6H5NHNH2; heating at 150-170°C and 0.01 Torr, 1 h; recrystn. in petroleum ether/benzene;

DOI:10.1039/j19660001590

Reference yield: 33.0%

phenylborondichloride (873-51-8) + phenylhydrazine (100-63-0) → Perhydro-1,3,4,6-tetraphenyl-1,2,4,5-tetra-aza-1,3-diborin (13831-67-9)

Guidance literature:

With triethylamine; In benzene; 3 h heating with reflux;

DOI:10.1039/j19660001590

Reference yield:

Bis-(dimethylamino)-phenylboran (1201-45-2) → Perhydro-1,3,4,6-tetraphenyl-1,2,4,5-tetra-aza-1,3-diborin (13831-67-9)

Guidance literature:

Multi-step reaction with 2 steps

1: xylene

In xylene;

upstream raw materials:

bis(phenylhydrazino)phenylborane

phenylborondichloride

phenylhydrazine

phenylbis(diethylamino)borane