chloro(1,2-bis(diphenylphosphino)benzene)(η5-cyclopentadienyl)ruthenium(II)

Base Information

Chemical Name:chloro(1,2-bis(diphenylphosphino)benzene)(η5-cyclopentadienyl)ruthenium(II)
CAS No.:610320-08-6
Molecular Formula:C₃₅H₂₉ClP₂Ru
Molecular Weight:648.086
Hs Code.:

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Chemical Property of chloro(1,2-bis(diphenylphosphino)benzene)(η5-cyclopentadienyl)ruthenium(II)

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Technology Process of chloro(1,2-bis(diphenylphosphino)benzene)(η5-cyclopentadienyl)ruthenium(II)

There total 1 articles about chloro(1,2-bis(diphenylphosphino)benzene)(η5-cyclopentadienyl)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 32993-05-8
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II)

: 13991-08-7
o-phenylenebis(diphenylphosphine)

: 610320-08-6
chloro(1,2-bis(diphenylphosphino)benzene)(η5-cyclopentadienyl)ruthenium(II)

: [(η5-cyclopentadienyl)Ru(triphenylphosphine)(η2-1,2-bis(diphenylphosphino)benzene)]Cl

Guidance literature:: In benzene; under N2; benzene added to mixt. of Ru complex and ligand (molar ratio 1:1); boiled for 24 h; cooled to room temp.; filtered; vol. of filtrate reduced, hexanes added, solvent removed by cannula, solid washed with hexanes, dried under vac. (Ru-Cl complex); ppt.after filtration washed with benzene and hexanes, dried under vac. (Ru- PPh3 complex); elem. anal.;
DOI:10.1021/om0303404

Reference yield: 48.0%

: 67-56-1
methanol

: 610320-08-6
chloro(1,2-bis(diphenylphosphino)benzene)(η5-cyclopentadienyl)ruthenium(II)

: 610320-06-4
(η5-cyclopentadienyl)Ru(η2-1,2-bis(diphenylphosphino)benzene)H

Guidance literature:: With Na; In methanol; Na (7.2 equiv.) added to suspn. of Ru complex in MeOH; boiled for 2 h; cooled to room temp.; solvent removed by cannula; solid washed with MeOH; dried under vac.; elem. anal.;
DOI:10.1021/om0303404