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Phosphonic acid, [1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-phenyl-1-propenyl]-, dimethyl ester, (E)-

Base Information Edit
  • Chemical Name:Phosphonic acid, [1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-phenyl-1-propenyl]-, dimethyl ester, (E)-
  • CAS No.:105762-54-7
  • Molecular Formula:C17H29O4PSi
  • Molecular Weight:356.474
  • Hs Code.:
  • Mol file:105762-54-7.mol
Phosphonic acid,
[1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-phenyl-1-propenyl]-, dimethyl
ester, (E)-

Synonyms:

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Chemical Property of Phosphonic acid, [1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-phenyl-1-propenyl]-, dimethyl ester, (E)- Edit
Chemical Property:
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MSDS Files:

SDS file from LookChem

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Technology Process of Phosphonic acid, [1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-phenyl-1-propenyl]-, dimethyl ester, (E)-

There total 5 articles about Phosphonic acid, [1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-phenyl-1-propenyl]-, dimethyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 4 steps
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 30 min, 2.) HMPA, 0 deg C, 18 h
2: 41 percent / H2O, Chloramine-T / methanol / 1.5 h / 0 - 25 °C
3: 1.) LDA / 1.) THF, -78 deg C, 2.) from 0 to 25 deg C, 5 min
4: 1.) LDA / 1.) Et2O, THF, -78 deg C, 5 min, 2.) a) 5 min, b) -50 deg C, 5 min
With n-butyllithium; water; chloroamine-T; lithium diisopropyl amide; In methanol;
DOI:10.1021/ja00170a026
Guidance literature:
Multi-step reaction with 3 steps
1: 41 percent / H2O, Chloramine-T / methanol / 1.5 h / 0 - 25 °C
2: 1.) LDA / 1.) THF, -78 deg C, 2.) from 0 to 25 deg C, 5 min
3: 1.) LDA / 1.) Et2O, THF, -78 deg C, 5 min, 2.) a) 5 min, b) -50 deg C, 5 min
With water; chloroamine-T; lithium diisopropyl amide; In methanol;
DOI:10.1021/ja00170a026
Guidance literature:
Multi-step reaction with 4 steps
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 30 min, 2.) HMPA, 0 deg C, 18 h
2: 41 percent / H2O, Chloramine-T / methanol / 1.5 h / 0 - 25 °C
3: 1.) LDA / 1.) THF, -78 deg C, 2.) from 0 to 25 deg C, 5 min
4: 1.) LDA / 1.) Et2O, THF, -78 deg C, 5 min, 2.) a) 5 min, b) -50 deg C, 5 min
With n-butyllithium; water; chloroamine-T; lithium diisopropyl amide; In methanol;
DOI:10.1021/ja00170a026
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