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dimethyl(phenylthio)bismuthane

Base Information
  • Chemical Name:dimethyl(phenylthio)bismuthane
  • CAS No.:96694-07-4
  • Molecular Formula:C8H11BiS
  • Molecular Weight:348.222
  • Hs Code.:
dimethyl(phenylthio)bismuthane

Synonyms:

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of dimethyl(phenylthio)bismuthane
Chemical Property:
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Technology Process of dimethyl(phenylthio)bismuthane

There total 1 articles about dimethyl(phenylthio)bismuthane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In diethyl ether; under exclusion of air and moisture (N2), addn. of Bi2Me4 to an ether soln. of Ph2S2 at 0°C, after 2 h at 0°C and 1 h at room temp. (exclusion of light) addn. of pentane, pptn. overnight on dry ice; filtered (dry ice cooled frit), repeatedly washed with ice-cold pentane, dried in vac.; elem. anal.;
Guidance literature:
In neat (no solvent); byproducts: (CH3)3Bi; react. at 90°C for 15 h in N2-stream; elem. anal.;
upstream raw materials:

tetramethyldibismuthane

diphenyldisulfane

Downstream raw materials:

Methyl-bis-(phenylthio)-bismutin

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