Methyl-bis-(phenylthio)-bismutin

Base Information

• Chemical Name: Methyl-bis-(phenylthio)-bismutin
• CAS No.: 28609-60-1
• Molecular Formula: C₁₃H₁₃BiS₂
• Molecular Weight: 442.359

Synonyms:Methyl-bis-(phenylthio)-bismutin

Chemical Property of Methyl-bis-(phenylthio)-bismutin

Chemical Property:

Purity/Quality:

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Technology Process of Methyl-bis-(phenylthio)-bismutin

There total 4 articles about Methyl-bis-(phenylthio)-bismutin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

trimethylbismuthine (593-91-9) + thiophenol (108-98-5) → Methyl-bis-(phenylthio)-bismutin (28609-60-1)

Guidance literature:

In benzene; 24 h;

DOI:10.1039/j29700000735

Reference yield: 80.0%

sodium ethanolate (141-52-6) + methyldibromobismuth(III) (60458-17-5) + thiophenol (108-98-5) → Methyl-bis-(phenylthio)-bismutin (28609-60-1) + sodium bromide (7647-15-6)

Guidance literature:

20°C, equiv. amt. of thiophenol; NaCl filtered off, the solvent evapd. in vac.;

Reference yield:

dimethyl(phenylthio)bismuthane (96694-07-4) → Methyl-bis-(phenylthio)-bismutin (28609-60-1)

Guidance literature:

In neat (no solvent); byproducts: (CH3)3Bi; react. at 90°C for 15 h in N2-stream; elem. anal.;

upstream raw materials:

trimethylbismuthine

thiophenol

dimethyl(phenylthio)bismuthane

sodium ethanolate

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