trans-2-bromo-1-(prop-2'-enyl-1'-oxy)cyclohexane

Base Information

Chemical Name:trans-2-bromo-1-(prop-2'-enyl-1'-oxy)cyclohexane
CAS No.:75681-57-1
Molecular Formula:C₉H₁₅BrO
Molecular Weight:219.121
Hs Code.:

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Chemical Property of trans-2-bromo-1-(prop-2'-enyl-1'-oxy)cyclohexane

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Technology Process of trans-2-bromo-1-(prop-2'-enyl-1'-oxy)cyclohexane

There total 1 articles about trans-2-bromo-1-(prop-2'-enyl-1'-oxy)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 107-18-6
allyl alcohol

: 110-83-8
cyclohexene

: 29840-04-8,75681-57-1
trans-2-bromo-1-(prop-2'-enyl-1'-oxy)cyclohexane

Guidance literature:: With N-Bromosuccinimide; 1) 0 deg C, 1 h, 2) room temperature, 3 h;
DOI:10.1016/S0040-4020(98)01137-5

Reference yield: 55.0%

: cobalt(II) chloride hexahydrate

: 29840-04-8,75681-57-1
trans-2-bromo-1-(prop-2'-enyl-1'-oxy)cyclohexane

: 95-45-4
butane-2,3-dione dioxime

: (Co(NC₅H₅)(C₄H₇N₂O₂)2(CH₂CHCH₂OC₆H₁₀))

: (7-oxabicyclo(4.3.0)non-9-yl)methylcobaloxime

Guidance literature:: With pyridine; sodium hydroxide; sodium tetrahydroborate; In methanol; water; to CoCl2*6H2O and dimethylglyoxime in MeOH added aq. NaOH, pyridine, mixt. stirred under N2 for 15 min at 0°C, treated with aq. NaOH and NaBH4 and stirred for 5 min, treated with 2-(allyloxy)cyclohexyl bromide and stirred for 4-6 h at room temp.; water added and mixt. extracted with benzene, ext. washed with water, dried over Na2SO4 and concd. under reduced pressure, residue chromd. on Florisil column with chloroform-ethylacetate (1:1) as eluent, solvent evapd.; elem. anal.;
DOI:10.1246/bcsj.55.1498