[Ni5(μ-N3)2(μ3-N3)2(μ-phenyl(2-pyridyl)ketoneoximato)(μ-CH3CO2)2(CH3OH)4]

Base Information

Chemical Name:[Ni5(μ-N3)2(μ3-N3)2(μ-phenyl(2-pyridyl)ketoneoximato)(μ-CH3CO2)2(CH3OH)4]
CAS No.:1255239-84-9
Molecular Formula:C₅₆H₅₈N₂₀Ni₅O₁₂
Molecular Weight:1496.65
Hs Code.:

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Chemical Property of [Ni5(μ-N3)2(μ3-N3)2(μ-phenyl(2-pyridyl)ketoneoximato)(μ-CH3CO2)2(CH3OH)4]

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Technology Process of [Ni5(μ-N3)2(μ3-N3)2(μ-phenyl(2-pyridyl)ketoneoximato)(μ-CH3CO2)2(CH3OH)4]

There total 2 articles about [Ni5(μ-N3)2(μ3-N3)2(μ-phenyl(2-pyridyl)ketoneoximato)(μ-CH3CO2)2(CH3OH)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 67-56-1
methanol

: sodium azide

: 6018-89-9
nickel(II) acetate tetrahydrate

: 1826-28-4
phenyl-2-pyridyl ketoxime

: 1255239-84-9
[Ni5(μ-N3)2(μ3-N3)2(μ-phenyl(2-pyridyl)ketoneoximato)(μ-CH3CO2)2(CH3OH)4]

Guidance literature:: In methanol; to a soln. of oxime-compound in CH3OH was added solid Ni-salt, stirred for 15 min, solid NaN3 was added in small portions, stirred for 10 min; layered with n-hexane-diethyl ether mixt. (1/1), crystals were filtered,washed with diethyl ether, dried under vac.; elem. anal.;
DOI:10.1021/ic1014829

Reference yield: 20.0%

: 67-56-1
methanol

: sodium azide

: nickel(II) perchlorate hexahydrate

: 127-09-3
sodium acetate

: 1826-28-4
phenyl-2-pyridyl ketoxime

: 1255239-84-9
[Ni5(μ-N3)2(μ3-N3)2(μ-phenyl(2-pyridyl)ketoneoximato)(μ-CH3CO2)2(CH3OH)4]

Guidance literature:: In methanol; to a soln. of oxime-compound in CH3OH was added solid Ni-salt, stirred for 15 min, solid NaN3 was added in small portions, stirred for 10 min; layered with n-hexane-diethyl ether mixt. (1/1), crystals were filtered,washed with diethyl ether, dried under vac.;
DOI:10.1021/ic1014829