(2-methoxycyclohexyl)phenyltellurium dibromide

Base Information

• Chemical Name: (2-methoxycyclohexyl)phenyltellurium dibromide
• CAS No.: 82486-31-5
• Molecular Formula: C₁₃H₁₈Br₂OTe
• Molecular Weight: 477.693
• Mol file: 82486-31-5.mol

Synonyms:

Chemical Property of (2-methoxycyclohexyl)phenyltellurium dibromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2-methoxycyclohexyl)phenyltellurium dibromide

There total 2 articles about (2-methoxycyclohexyl)phenyltellurium dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

methanol (67-56-1) + diphenyl ditelluride (32294-60-3) + cyclohexene (110-83-8) → (2-methoxycyclohexyl)phenyltellurium dibromide (82486-31-5,92693-26-0)

Guidance literature:

With bromine; at 100 ℃; for 1h;

DOI:10.1016/0022-328X(83)85051-7

Reference yield: 65.0%

methanol (67-56-1) + phenyltellurium tribromide (36309-64-5) + cyclohexene (110-83-8) → (2-methoxycyclohexyl)phenyltellurium dibromide (82486-31-5,92693-26-0)

Guidance literature:

With bromine; at 65 ℃; for 1h;

DOI:10.1016/0022-328X(83)85051-7

Reference yield: 100.0%

(2-methoxycyclohexyl)phenyltellurium dibromide (82486-31-5,92693-26-0) → (2-Methoxy-cyclohexyltellanyl)-benzene (82486-24-6)

Guidance literature:

With hydrazine hydrate; In ethanol; Ambient temperature;

DOI:10.1016/0022-328X(83)85051-7

upstream raw materials:

methanol

diphenyl ditelluride

cyclohexene

phenyltellurium tribromide

Downstream raw materials:

(2-Methoxy-cyclohexyltellanyl)-benzene

C₁₃H₁₈O₂Te

2-methoxycyclohexyl phenyl telluroxide hydrate

3-methoxycyclohexene

Refernces

• 1、 Uemura, Sakae,Fukuzawa, Shin-ichi. "New Aspects of the Telluroxide Elimination. A Facile Elimination of sec-Alkyl Phenyl Telluroxide Leading to Olefins, Allylic Alcohols, and Allylic Ethers". . p. 2748 - 2752. Retrieved 2007/10/02.