6-benzyloxy-4-cyano-4-ethoxycarbonyl-1,2,3,4-tetrahydro-2-amino methylene>carbazole

Base Information

Chemical Name:6-benzyloxy-4-cyano-4-ethoxycarbonyl-1,2,3,4-tetrahydro-2-amino methylene>carbazole
CAS No.:131920-03-1
Molecular Formula:C₃₃H₂₉N₃O₆
Molecular Weight:563.61
Hs Code.:

6-benzyloxy-4-cyano-4-ethoxycarbonyl-1,2,3,4-tetrahydro-2-<N-<2-(methoxycarbonyl)-benzoyl>amino methylene>carbazole

Synonyms:

Suppliers and Price of 6-benzyloxy-4-cyano-4-ethoxycarbonyl-1,2,3,4-tetrahydro-2-amino methylene>carbazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-benzyloxy-4-cyano-4-ethoxycarbonyl-1,2,3,4-tetrahydro-2-amino methylene>carbazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-benzyloxy-4-cyano-4-ethoxycarbonyl-1,2,3,4-tetrahydro-2-amino methylene>carbazole

There total 6 articles about 6-benzyloxy-4-cyano-4-ethoxycarbonyl-1,2,3,4-tetrahydro-2-amino methylene>carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 67-56-1
methanol

: 131920-02-0
6-benzyloxy-4-cyano-4-ethoxycarbonyl-1H-2,3-dihydro-1-(N-phthalimidyl methylene)carbazole

: 131920-03-1
6-benzyloxy-4-cyano-4-ethoxycarbonyl-1,2,3,4-tetrahydro-2-amino methylene>carbazole

Guidance literature:: With toluene-4-sulfonic acid; for 24h;
DOI:10.1016/S0040-4020(01)88387-3

Reference yield: 25.0%

: 131920-02-0
6-benzyloxy-4-cyano-4-ethoxycarbonyl-1H-2,3-dihydro-1-(N-phthalimidyl methylene)carbazole

: 131920-03-1
6-benzyloxy-4-cyano-4-ethoxycarbonyl-1,2,3,4-tetrahydro-2-amino methylene>carbazole

: 131920-15-5
6-benzyloxy-4-cyano-4-ethoxycarbonyl-1,2,3,4-tetrahydro-1-amino methylene>carbazole

Guidance literature:: With hydrazine hydrate; In methanol; for 0.25h; Heating;
DOI:10.1016/S0040-4020(01)88387-3

Reference yield:

: 19667-37-9,34839-11-7,148857-42-5,148857-44-7
2-(3-chloro-2-hydroxypropyl)-1H-isoindole-1,3(2H)-dione

: 131920-03-1
6-benzyloxy-4-cyano-4-ethoxycarbonyl-1,2,3,4-tetrahydro-2-amino methylene>carbazole

Guidance literature:: Multi-step reaction with 5 steps

1: 48 percent / CrO₃/H₂O/conc. H₂SO₄ / acetone / 0.75 h / Ambient temperature

2: 1.) NaH / 1.) DMF, rt, 30 min, 2.) to rt, 4 h

3: 80 percent / DMAD / tetrahydrofuran / 3.5 h / Ambient temperature

4: 4-toluenesulphonic acid / toluene / 0.5 h / Heating

5: 93 percent / 4-toluenesulphonic acid / 24 h

With chromium(VI) oxide; sulfuric acid; water; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; acetone; toluene;
DOI:10.1016/S0040-4020(01)88387-3