7-Benzyloxy-1-(5-benzyloxy-2-methoxy-benzyl)-6-methoxy-2-((S)-1-phenyl-ethyl)-3,4-dihydro-isoquinolinium

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Chemical Name:7-Benzyloxy-1-(5-benzyloxy-2-methoxy-benzyl)-6-methoxy-2-((S)-1-phenyl-ethyl)-3,4-dihydro-isoquinolinium
CAS No.:192190-42-4
Molecular Formula:C₄₀H₄₀NO₄
Molecular Weight:598.762
Hs Code.:

Synonyms:

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Chemical Property of 7-Benzyloxy-1-(5-benzyloxy-2-methoxy-benzyl)-6-methoxy-2-((S)-1-phenyl-ethyl)-3,4-dihydro-isoquinolinium

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Technology Process of 7-Benzyloxy-1-(5-benzyloxy-2-methoxy-benzyl)-6-methoxy-2-((S)-1-phenyl-ethyl)-3,4-dihydro-isoquinolinium

There total 8 articles about 7-Benzyloxy-1-(5-benzyloxy-2-methoxy-benzyl)-6-methoxy-2-((S)-1-phenyl-ethyl)-3,4-dihydro-isoquinolinium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 192190-41-3
N-[2-(4-benzyloxy-3-methoxyphenyl)ethyl]-N-((S)-1-phenylethyl)-2-(5-benzyloxy-2-methoxyphenyl)acetamide

: 192190-42-4
7-Benzyloxy-1-(5-benzyloxy-2-methoxy-benzyl)-6-methoxy-2-((S)-1-phenyl-ethyl)-3,4-dihydro-isoquinolinium

Guidance literature:: With trichlorophosphate; In toluene; for 3.5h; Heating;
DOI:10.3987/com-97-7782

Reference yield:

: 52329-05-2
5-benzyloxy-2-methoxyphenyl methanol

: 192190-42-4
7-Benzyloxy-1-(5-benzyloxy-2-methoxy-benzyl)-6-methoxy-2-((S)-1-phenyl-ethyl)-3,4-dihydro-isoquinolinium

Guidance literature:: Multi-step reaction with 6 steps

1: 87.4 percent / SOCl₂, N,N-dimethylaniline / benzene / 1 h / 100 °C

2: 95.1 percent / dimethylsulfoxide / 1 h / 40 - 50 °C

3: 84.9 percent / 25percent ethanolic KOH / bis-(2-hydroxy-ethyl) ether / 21 h

4: SOCl₂ / benzene

5: 88.9 percent / 5percent aq. Na₂CO₃ / diethyl ether / 2 h / 0 - 5 °C

6: POCl₃ / toluene / 3.5 h / Heating

With potassium hydroxide; thionyl chloride; sodium carbonate; N,N-dimethyl-aniline; trichlorophosphate; In diethyl ether; dimethyl sulfoxide; toluene; diethylene glycol; benzene;
DOI:10.3987/com-97-7782

Reference yield:

: 54313-35-8
2-(4-(benzyloxy)-3-methoxyphenyl)acetyl chloride

: 192190-42-4
7-Benzyloxy-1-(5-benzyloxy-2-methoxy-benzyl)-6-methoxy-2-((S)-1-phenyl-ethyl)-3,4-dihydro-isoquinolinium

Guidance literature:: Multi-step reaction with 4 steps

1: 82.8 percent / 5percent aq. Na₂CO₃ / diethyl ether / 1 h / 0 - 5 °C

2: 87 percent / 47percent BF₃*ether, 1.0M BH₃*THF / tetrahydrofuran / 2.5 h / 70 °C

3: 88.9 percent / 5percent aq. Na₂CO₃ / diethyl ether / 2 h / 0 - 5 °C

4: POCl₃ / toluene / 3.5 h / Heating

With borane-THF; boron trifluoride diethyl etherate; sodium carbonate; trichlorophosphate; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.3987/com-97-7782