6-Oxo-1-phenyl-4-{N'-[1-phenyl-meth-(Z)-ylidene]-hydrazino}-1,6-dihydro-pyridazine-3-carboxylic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Base Information

• Chemical Name: 6-Oxo-1-phenyl-4-{N'-[1-phenyl-meth-(Z)-ylidene]-hydrazino}-1,6-dihydro-pyridazine-3-carboxylic acid [1-phenyl-meth-(E)-ylidene]-hydrazide
• CAS No.: 129109-39-3
• Molecular Formula: C₂₅H₂₀N₆O₂
• Molecular Weight: 436.473
• Mol file: 129109-39-3.mol

Synonyms:

Chemical Property of 6-Oxo-1-phenyl-4-{N'-[1-phenyl-meth-(Z)-ylidene]-hydrazino}-1,6-dihydro-pyridazine-3-carboxylic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-Oxo-1-phenyl-4-{N'-[1-phenyl-meth-(Z)-ylidene]-hydrazino}-1,6-dihydro-pyridazine-3-carboxylic acid [1-phenyl-meth-(E)-ylidene]-hydrazide

There total 3 articles about 6-Oxo-1-phenyl-4-{N'-[1-phenyl-meth-(Z)-ylidene]-hydrazino}-1,6-dihydro-pyridazine-3-carboxylic acid [1-phenyl-meth-(E)-ylidene]-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

5-Hydrazino-3-oxo-2-phenyl-2,3-dihydropyridazine-6-carboxylic hydrazide (129109-53-1) + benzaldehyde (100-52-7) → 6-Oxo-1-phenyl-4-{N'-[1-phenyl-meth-(Z)-ylidene]-hydrazino}-1,6-dihydro-pyridazine-3-carboxylic acid [1-phenyl-meth-(E)-ylidene]-hydrazide (129109-39-3)

Guidance literature:

In ethanol; for 0.166667h; Heating;

Reference yield:

methyl 5-chloro-3-oxo-2-phenyl-2,3-dihydropyridazine-6-carboxylate (129109-17-7) → 6-Oxo-1-phenyl-4-{N'-[1-phenyl-meth-(Z)-ylidene]-hydrazino}-1,6-dihydro-pyridazine-3-carboxylic acid [1-phenyl-meth-(E)-ylidene]-hydrazide (129109-39-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 84 percent / N₂H₄*H₂O / ethanol / 0.25 h / Heating

2: 100 percent / ethanol / 0.17 h / Heating

With hydrazine hydrate; In ethanol;

Reference yield:

methyl 2-phenyl-5-hydroxy-3-oxo-2,3-dihydropyridazine-6-carboxylate (121582-53-4) → 6-Oxo-1-phenyl-4-{N'-[1-phenyl-meth-(Z)-ylidene]-hydrazino}-1,6-dihydro-pyridazine-3-carboxylic acid [1-phenyl-meth-(E)-ylidene]-hydrazide (129109-39-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 91 percent / POCl₃ / 3 h / 95 - 100 °C

2: 84 percent / N₂H₄*H₂O / ethanol / 0.25 h / Heating

3: 100 percent / ethanol / 0.17 h / Heating

With hydrazine hydrate; trichlorophosphate; In ethanol;

upstream raw materials:

5-Hydrazino-3-oxo-2-phenyl-2,3-dihydropyridazine-6-carboxylic hydrazide

benzaldehyde

methyl 5-chloro-3-oxo-2-phenyl-2,3-dihydropyridazine-6-carboxylate

methyl 2-phenyl-5-hydroxy-3-oxo-2,3-dihydropyridazine-6-carboxylate