[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]Ta(CH₂-t-Bu)Cl₂

Base Information

Chemical Name:[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]Ta(CH₂-t-Bu)Cl₂
CAS No.:919479-92-8
Molecular Formula:C₂₂H₂₆Cl₂F₆N₃Ta
Molecular Weight:698.313
Hs Code.:

[(3,4,5-F<sub>3</sub>C<sub>6</sub>H<sub>2</sub>NCH<sub>2</sub>CH<sub>2</sub>)2NMe]Ta(CH<sub>2</sub>-t-Bu)Cl<sub>2</sub>

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Chemical Property of [(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]Ta(CH₂-t-Bu)Cl₂

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Technology Process of [(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]Ta(CH₂-t-Bu)Cl₂

There total 1 articles about [(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]Ta(CH₂-t-Bu)Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 919479-87-1
[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]TaCl₃

: 13132-23-5
2,2-dimethylpropylmagnesium chloride

: 919479-92-8
[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]Ta(CH₂-t-Bu)Cl₂

Guidance literature:: In diethyl ether; Mg compd. in Et2O added to a cooled suspn. of Ta complex, allowed to warm to room temp. and stirred for 3 h; 1,4-dioxane added, stirred for 10 min, filtered, washed (Et2O), evapd. (vac.), triturated with pentane, collected on a frit, washed (pentane), dried (vac.); elem. anal.;
DOI:10.1016/j.ica.2006.03.044

Reference yield: 73.0%

: 919479-92-8
[(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]Ta(CH₂-t-Bu)Cl₂

: 676-58-4
methylmagnesium chloride

: [(3,4,5-F₃C₆H₂NCH₂CH₂)2NMe]Ta(CH-t-Bu)(CH₃)

Guidance literature:: In tetrahydrofuran; diethyl ether; CH3MgCl in THF added dropwise to a suspn. of Ta complex in Et2O at -30°C, reacted for 1 h; 1,4-dioxane added, stirred for 10 min, filtered, rinsed with ether, evapd., triturated with pentane, filtered off, washed (pentane), dried (vac.); elem. anal.;
DOI:10.1016/j.ica.2006.03.044