2-(3,5-Dinitrobenzene-1-sulfonyl)ethan-1-ol

Base Information

Chemical Name:2-(3,5-Dinitrobenzene-1-sulfonyl)ethan-1-ol
CAS No.:105897-14-1
Molecular Formula:C8H8N2O7S
Molecular Weight:276.227
Hs Code.:
DSSTox Substance ID:DTXSID00542657
Wikidata:Q82419388

Synonyms:105897-14-1;2-(3,5-Dinitrobenzene-1-sulfonyl)ethan-1-ol;DTXSID00542657

Suppliers and Price of 2-(3,5-Dinitrobenzene-1-sulfonyl)ethan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(3,5-Dinitrobenzene-1-sulfonyl)ethan-1-ol

Chemical Property:

XLogP3:0.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:3
Exact Mass:276.00522177
Heavy Atom Count:18
Complexity:396

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C=C1[N+](=O)[O-])S(=O)(=O)CCO)[N+](=O)[O-]

Technology Process of 2-(3,5-Dinitrobenzene-1-sulfonyl)ethan-1-ol

There total 5 articles about 2-(3,5-Dinitrobenzene-1-sulfonyl)ethan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.4%

: 75-21-8,99932-75-9
oxirane

: 28084-45-9
3,5-dinitro-benzenesulfonic acid

: 105897-14-1
2-(3,5-dinitrophenylsulfonyl)ethanol

Guidance literature:: at 40 ℃; for 2h; pH=7.5 - 8;

Reference yield: 63.0%

: 105897-13-0
2-(3,5-dinitrophenylthio)ethanol

: 105897-14-1
2-(3,5-dinitrophenylsulfonyl)ethanol

Guidance literature:: With dihydrogen peroxide; In trifluoroacetic acid; for 1.5h; Heating;

Reference yield:

: 99-35-4
1,3,5-trinitrobenzene

: 105897-14-1
2-(3,5-dinitrophenylsulfonyl)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium / 1.) tert-butyl alcohol, 2.) DMSO, room temperature, 24 h; 50 deg C, 1 h

2: 63 percent / 30percent hydrogen peroxide / trifluoroacetic acid / 1.5 h / Heating

With dihydrogen peroxide; potassium; In trifluoroacetic acid;