Technology Process of N,N-dimethyl-3-(3-methoxyphenylthio)-2-thenylamine
There total 5 articles about N,N-dimethyl-3-(3-methoxyphenylthio)-2-thenylamine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; boron trifluoride diethyl etherate;
In
tetrahydrofuran;
Yield given;
1.) 1 h, 2.) reflux, 4 h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 61 percent / K2CO3, Cu / dimethylformamide / 13 h / Heating
2: 1.) 7percent BuLi / 1.) ether, hexane, -60 deg C, 1.5 h
3: SOCl2 / benzene / 2 h / Heating
4: benzene; H2O / 5 h / Ambient temperature
5: NaBH4, BF3*O(C2H5)2 / tetrahydrofuran / 1.) 1 h, 2.) reflux, 4 h
With
sodium tetrahydroborate; n-butyllithium; thionyl chloride; boron trifluoride diethyl etherate; copper; potassium carbonate;
In
tetrahydrofuran; water; N,N-dimethyl-formamide; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) 7percent BuLi / 1.) ether, hexane, -60 deg C, 1.5 h
2: SOCl2 / benzene / 2 h / Heating
3: benzene; H2O / 5 h / Ambient temperature
4: NaBH4, BF3*O(C2H5)2 / tetrahydrofuran / 1.) 1 h, 2.) reflux, 4 h
With
sodium tetrahydroborate; n-butyllithium; thionyl chloride; boron trifluoride diethyl etherate;
In
tetrahydrofuran; water; benzene;
