C₆H₄OCHNC₆H₃(CH(CH₃)2)2Ni(CO)COCH₃

Base Information

Chemical Name:C₆H₄OCHNC₆H₃(CH(CH₃)2)2Ni(CO)COCH₃
CAS No.:1305337-29-4
Molecular Formula:C₂₂H₂₅NNiO₃
Molecular Weight:410.135
Hs Code.:

C<sub>6</sub>H<sub>4</sub>OCHNC<sub>6</sub>H<sub>3</sub>(CH(CH<sub>3</sub>)2)2Ni(CO)COCH<sub>3</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆H₄OCHNC₆H₃(CH(CH₃)2)2Ni(CO)COCH₃

Chemical Property:

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Technology Process of C₆H₄OCHNC₆H₃(CH(CH₃)2)2Ni(CO)COCH₃

There total 5 articles about C₆H₄OCHNC₆H₃(CH(CH₃)2)2Ni(CO)COCH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17972-13-3,29086-13-3,53699-34-6
p-methylbenzylidene-methylamine

: 187605-57-8,1056566-19-8
2-[(2,6-diisopropylphenyl)iminomethyl]phenol

: 1305337-29-4
C₆H₄OCHNC₆H₃(CH(CH₃)2)2Ni(CO)COCH₃

: 2-((2,6-diisopropylphenyl)iminomethyl)phenoxide)Ni(COCH₃)(N-methyltolualdimine)

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: CH₃C₆H₄CHNCH₃ / benzene-d6

With CH₃C₆H₄CHNCH₃; In benzene-d6; benzene;
DOI:10.1016/j.ica.2010.12.024

Reference yield:

: 3230-65-7
3,4-dihydroisoquinoline

: 187605-57-8,1056566-19-8
2-[(2,6-diisopropylphenyl)iminomethyl]phenol

: 1305337-29-4
C₆H₄OCHNC₆H₃(CH(CH₃)2)2Ni(CO)COCH₃

: 1305337-25-0
(2-((2,6-diisopropylphenyl)iminomethyl)phenoxide)Ni(COCH₃)(3,4-dihydroisoquinoline)

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: C₉H₉N / benzene-d6

With C₉H₉N; In benzene-d6; benzene;
DOI:10.1016/j.ica.2010.12.024

Reference yield:

: 201230-82-2
carbon monoxide

: (2-((2,6-diisopropylphenyl)iminomethyl)phenoxide)Ni(CH₃)(N-methyltolualdimine)

: 1305337-29-4
C₆H₄OCHNC₆H₃(CH(CH₃)2)2Ni(CO)COCH₃

: 2-((2,6-diisopropylphenyl)iminomethyl)phenoxide)Ni(COCH₃)(N-methyltolualdimine)

Guidance literature:: With CH₃C₆H₄CHNCH₃; In benzene-d6; Ni complex and imine (1:3) in C6D6 reacted under 1 aym. of CO at room temp. for 15 min; not isolated, detcd. by NMR;
DOI:10.1016/j.ica.2010.12.024