[(Ph₂CH)(C₅H₉)2PH][HB(p-C₆F₄H)3]

Base Information

Chemical Name:[(Ph₂CH)(C₅H₉)2PH][HB(p-C₆F₄H)3]
CAS No.:1239667-62-9
Molecular Formula:C₁₈H₄BF₁₂*C₂₃H₂₉P*H
Molecular Weight:796.487
Hs Code.:

[(Ph<sub>2</sub>CH)(C<sub>5</sub>H<sub>9</sub>)2PH][HB(p-C<sub>6</sub>F<sub>4</sub>H)3]

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Chemical Property of [(Ph₂CH)(C₅H₉)2PH][HB(p-C₆F₄H)3]

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Technology Process of [(Ph₂CH)(C₅H₉)2PH][HB(p-C₆F₄H)3]

There total 3 articles about [(Ph₂CH)(C₅H₉)2PH][HB(p-C₆F₄H)3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1559-88-2
1-bromo-2,3,5,6-tetrafluorobenzene

: 1239667-62-9
[(Ph₂CH)(C₅H₉)2PH][HB(p-C₆F₄H)3]

Guidance literature:: Multi-step reaction with 3 steps

1: (CH₃)2CHMgCl / diethyl ether

2: not given

3: hexane

With (CH₃)2CHMgCl; In diethyl ether; hexane;
DOI:10.1021/om100563m

Reference yield:

: 1094249-93-0
(Et₂O)B(p-C₆F₄H)3

: 1239667-62-9
[(Ph₂CH)(C₅H₉)2PH][HB(p-C₆F₄H)3]

Guidance literature:: Multi-step reaction with 2 steps

1: not given

2: hexane

In hexane;
DOI:10.1021/om100563m

Reference yield:

: 148892-95-9
tris(2,3,5,6-tetrafluorophenyl)borane triethylphosphine oxide

: 1239667-58-3
(Ph₂CH)(C₅H₉)2P

: 1333-74-0
hydrogen

: 1239667-62-9
[(Ph₂CH)(C₅H₉)2PH][HB(p-C₆F₄H)3]

Guidance literature:: In hexane; High Pressure; (N2); mixing hexane soln. of phosphine deriv. and borane deriv. in C6H5Br, freezing at -196°C, exposure to H2, warming to room temp., stirring overnight; pressure of H2 after warming to room temp. was 4 atm; evapn., recrystn. by addn. of hexanes to concd. CH2Cl2 soln. and keepingat -35°C for wk, elem. anal.;
DOI:10.1021/om100563m